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50 and more essential NMR experiments : a detailed guide

Author: Matthias Findeisen; Stefan Berger
Publisher: Weinheim, Germany : Wiley-VCH, [2014]
Edition/Format:   Print book : EnglishView all editions and formats

This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special  Read more...


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Document Type: Book
All Authors / Contributors: Matthias Findeisen; Stefan Berger
ISBN: 9783527334834 3527334831
OCLC Number: 862345842
Description: 308 pages : illustrations (some color) ; 24 cm
Contents: PREFACE THE ORGANIC SET OF NMR SPECTRA The 1H NMR Experiment APT-13C NMR COSY NOESY HSQC HMBC ADVANCED ORGANIC NMR SPECTROSCOPY 2D J-Resolved 1H NMR Spectroscopy ROESY TOCSY HSQC-TOCSY HOESY INADEQUATE ADEQUATE J-HMBC Gated Decoupling SELECTIVE METHODS Water suppression by Presaturation Solvent Suppression by 1D-NOESY Water Suppression by SOGGY Excitation Sculpting Solvent Suppression using WET SELTOCSY SELNOESY SELINCOR SELINQUATE Band Selective HMBC HETERONUCLEAR NMR 11B NMR Spectroscopy 15N NMR Spectroscopy 17O NMR Spectroscopy 19F NMR Spectroscopy 29Si NMR Spectroscopy 57Fe NMR Spectroscopy 195Pt NMR Spectroscopy EXPERIMENTS IN PHYSICAL ORGANIC CHEMISTRY Measurement of the Spin - Lattice Relaxation Time T1 Measurement of the Spin - Spin Relaxation Time T2 Dynamic 1H NMR Spectroscopy Diffusion Measurement with DOSY Residual Dipolar Couplings (RDC) ORGANIC CHEMISTRY APPLICATIONS ASIS Chirality Determination Advanced Mosher Method Quantitative NMR and Relaxation Reagents Determination of Association Constants Ka STD NMR A Kinetic Experiment AN EXCURSION TO THE SOLID STATE AND TO STRUCTURAL BIOLOGY The CP/MAS Experiment High-Resolution Magic-Angle Spinning HN-HSQC HNCA MAINTENANCE AND CALIBRATION Calibration of Pulse Duration in the Transmitter Channel Calibration of the Pulse Duration in the Indirect Channel Shaped Pulses Adiabatic pulses Temperature Calibration in NMR Calibration of Pulsed Field Gradients APPENDIX Answers Pulse Programs Elementary Product Operator Formalism Rules Chemical Shift and Spin-Coupling Data for Strychnine Picture Credits INDEX
Other Titles: Fifty and more essential NMR experiments
Responsibility: Matthias Findeisen, Stefan Berger.
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