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Basic gas chromatography-mass spectrometry : principles and techniques

Author: Francis W Karasek; R E Clement
Publisher: Amsterdam ; New York : Elsevier ; New York, NY, U.S.A. : Distributors for the U.S. and Canada, Elsevier Science Pub. Co., ©1988.
Edition/Format:   Print book : EnglishView all editions and formats
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Covering the basic principles of both gas chromatography (GC) and mass spectrometry (MS) to the extent necessary to understand and deal with the data generated in a GC-MS analysis. This book focuses  Read more...

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Genre/Form: Einführung
Additional Physical Format: Online version:
Karasek, Francis W., 1919-
Basic gas chromatography-mass spectrometry.
Amsterdam ; New York : Elsevier ; New York, NY, U.S.A. : Distributors for the U.S. and Canada, Elsevier Science Pub. Co., ©1988
(OCoLC)645673604
Material Type: Internet resource
Document Type: Book, Internet Resource
All Authors / Contributors: Francis W Karasek; R E Clement
ISBN: 0444427600 9780444427601
OCLC Number: 17326982
Description: 201 pages : illustrations ; 25 cm
Contents: 1. Introduction. An overview. Computerization. 2. Gas Chromatography. Fundamentals. Van Deemter equation: significance, evaluation. Columns: packed columns, wall-coated open tubular columns. Detectors: thermal conductivity detector, flame ionization detector, electron capture detector. Analysis techniques: sample injection, temperature programming, retention index. Instrumentation: computerization, data acquisition and analysis. Suggested reading. 3. Mass Spectrometry. Fundamentals: electron ionization, chemical ionization. Instrumentation: quadrupole mass spectrometers, magnetic sector mass spectrometers. Interpretation of mass spectra: types of ions, isotopic abundances and characteristic ion clusters, nitrogen rule and rings-plus-double-bonds, steps in interpretation, examples, problems. Suggested reading. 4. Gas Chromatography-Mass Spectrometry. Vacuum and gas flow: basic principles, analysis of vacuum and gas flow, interfaces. Computerization: computerized operation, characteristics. Data analysis: reconstructed gas chromatogram, mass chromatogram, selected ion monitoring, background subtraction, Biller-Biemann stripping technique. Compound identification using reference spectra matching: mass spectral compilations, methods of computerized mass spectral search, commercial mass spectral computer search systems. Quantitative analysis by selected ion monitoring: choice of ions, magnetic versus quadrupole analyzers, identification and quantitation procedures, use of isotopically labelled compounds, precision, accuracy, and limit of detection. Automated GC-MS operation: automated data acquisition, automated data analysis, total automated analysis. GC-MS-computer instrumentation: Finnigan MAT systems, Hewlett-Packard systems. Suggested reading. 5. GC-MS-Computer Applications. Analysis of chlorinated dibenzo-p-dioxins and dibenzofurans: incinerator emissions, biological samples, summary and conclusions. Use of high performance liquid chromatography for complex mixture analysis: HPLC fractionation of the mixture into compound types. Use of high resolution GC-MS for identity confirmation. New developments: MS-MS: description of the technique, scan techniques, instrumental configurations, comparison of GC-MS and MS-MS. Suggested reading. 6. Glossary. Subject Index.
Responsibility: F.W. Karasek and R.E. Clement.
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