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Characterization and design of zeolite catalysts : solid acidity, shape selectivity and loading properties

Author: Miki Niwa; Naonobu Katada; Kazu Okumura
Publisher: Heidelberg ; New York : Springer-Verlag, ©2010.
Series: Springer series in materials science, v. 141.
Edition/Format:   eBook : Document : EnglishView all editions and formats
Summary:

Catalysts based on these microporous, aluminosilicate minerals are used by chemical companies in the interconversion of hydrocarbons and the alkylation of aromatic compounds. This book characterizes  Read more...

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Genre/Form: Electronic books
Additional Physical Format: Print version:
Niwa, Miki.
Characterization and design of zeolite catalysts
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: Miki Niwa; Naonobu Katada; Kazu Okumura
ISBN: 9783642126208 3642126200
OCLC Number: 668082976
Description: 1 online resource (x, 184 pages) : illustrations (some color).
Contents: Note continued: 3.6. Distorted Structure of Zeolite and Related Material with Lewis Acidity and Broad Distribution of Acid Strength --
3.7. Measurements of Metal Oxide Overlayer --
3.8. Extinction Coefficients of NH4 + and NH3 Adsorbed on Brønsted and Lewis Acid Sites, Respectively --
References --
4. DFT Calculation of the Solid Acidity --
4.1. DFT Calculation --
4.1.1. DFT Calculation Applied to the Study on Brønsted Acidity --
4.1.2. Embedded Cluster and Periodic Boundary Conditions --
4.2. Application to Chabazite, a Simple Zeolite --
4.2.1. Brønsted Acid Sites in Chabazite Based on the Models Within the Periodic Boundary Conditions --
4.2.2. Brønsted Acid Site in an Embedded Cluster Model --
4.3. Application to Other Zeolites --
4.3.1. FAU, MOR, and BEA Calculated Under the Conditions of the Embedded Cluster and the Periodic Boundary --
4.3.2. MFI, FER, and MWW Calculated Under the Embedded Cluster Model --
4.4. Modified Zeolites --
4.4.1. Divalent Cation-Exchanged Y Zeolites Based on the Embedded Cluster Model --
4.4.2. Modified Brønsted OH in Y Zeolite Based on the Periodic Boundary Conditions --
4.5. Dependence of Brønsted Acid Strength on Local Geometry --
References --
5. Catalytic Activity and Adsorption Property --
5.1. Paraffin Cracking --
5.1.1. Evaluation of Intrinsic Activity of Acid Site --
5.1.2. Dependence of Activity on Acid Strength --
5.1.3. Thermodynamic Description on Correlation Between Activation Energy and Ammonia Desorption Heat --
5.1.4. Behavior of Acid Sites in 8- and 12-Rings of Mordenite --
5.2. Adsorption of Aromatic Hydrocarbons --
5.3. Friedel-Crafts Alkylation on Ga-MCM-41 --
5.4. Amination of Phenol into Aniline on Ga/ZSM-5 --
References --
6. CVD of Silica for the Shape Selective Reaction --
6.1. Reactants and Products Shape Selectivity, Concept and Definition. Note continued: 6.2. Chemical Vapor Deposition of Silica and the Procedure --
6.3. Formation of Silica Overlayer on the External Surface --
6.3.1. Method of Benzene-Filled Pore for the Measurement of External Surface Area --
6.3.2. Mechanism of CVD to form the Silica Overlayer --
6.3.3. Formation of Silica Overlayer on Zeolite and Metal Oxide, and Its Function --
6.4. Fine Control of Pore-Opening Size --
6.4.1. Mordenite --
6.4.2. MFI Zeolite --
6.4.3. Zeolite --
6.4.4. Y Zeolite --
6.5. Characterization of Deposited Oxide --
6.5.1. XPS Measurements --
6.5.2. EXAFS of the Deposited Germanium --
6.5.3. TEM Observation --
6.6. External Surface Acidity: Measurements and Inactivation --
References --
7. Application of the CVD of Silica to the Shape Selective Reaction --
7.1. Selective Formation of Para-Dialkylbenzene --
7.1.1. Principle of the Shape Selectivity --
7.1.2. CVD Zeolite to Produce the Para-Dialkylbenzene --
7.1.3. In Situ Production of CVD Zeolites --
7.1.4. HZSM-5 In Situ and Ex Situ Prepared for the CVD of Silicon Alkoxide --
7.1.5. CLD of Silica for the Shape Selective Adsorption --
7.2. Selective Cracking of Linear Alkane (Dewaxing) --
7.3. Various Applications --
7.3.1. Preferential Production of Dimethylamine from Methanol and Ammonia --
7.3.2. Improvement of the Life and the Activity of Catalysts --
7.3.3. Selective Removal of Undesired Products --
7.3.4. Applications to Zeolites from Various View-Points --
References --
8. Zeolite Loading Property for Active Sites and XAFS Measurements --
8.1. EXAFS and XANES Measurements of Loaded Metals --
8.1.1. DXAFS and QXAFS Analysis --
8.1.2. Formation of Molecular-Like PdO Through the Interaction with Acid Sites of Zeolites --
8.1.3. Reversible Cluster Formation Through the Interaction with Acid Sites of Zeolites. Note continued: 8.2. In Situ QXAFS Studies on the Dynamic Coalescence and Dispersion Processes of Pd in USY Zeolite --
8.3. Formation of the Atomically Dispersed Pd0 Through H2 Bubbling in o-Xylene: XAFS Measurements of Metals in the Liquid --
References --
9. Catalytic Reaction on the Palladium-Loaded Zeolites --
9.1. Combustion of Hydrocarbons Over Pd-Supported Catalysts --
9.1.1. Toluene Combustion --
9.1.2. Methane Combustion --
9.2. Selective Reduction of NO with Methane in the Presence of Oxygen --
9.2.1. Improvement in the Activity Derived by the Combined Effect of Adsorbent of Aromatic Acids --
9.3. Cross-Coupling Reactions Over Pd Loaded on FAU-Type Zeolites --
9.3.1. Heck Coupling Reactions Over Pd Loaded on H-Y Zeolites --
9.3.2. Remarkable Enhancement of Catalytic Activity Induced by the H2 Bubbling in Suzuki-Miyaura Coupling Reactions --
9.3.3. Possible Mechanism for the Formation of Active Pd Species in o-Xylene --
References.
Series Title: Springer series in materials science, v. 141.
Responsibility: Miki Niwa, Naonobu Katada, Kazu Okumura.

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