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Preface. Foreword. Symbols and Acronyms. 1 Introduction - An Overview of Practical Electrochemistry. Practical Hints. Electrodes. Measuring Instruments. Electrochemical Cells. Data Recording. 2 Electrochemistry in Equilibrium. Experiment 2.1: The Electrochemical Series. Experiment 2.2: Standard Electrode Potentials and the Mean Activity Coefficient. Experiment 2.3: pH-Measurements and Potentiometrically Indicated Titrations. Experiment 2.4: Redox Titrations (Cerimetry). Experiment 2.5: Differential Potentiometric Titration. Experiment 2.6: Potentiometric Measurement of the Kinetics of the Oxidation of Oxalic Acid. Experiment 2.7: Polarization and Decomposition Voltage. 3 Electrochemistry with Flowing Current. Experiment 3.1: Ion Movement in an Electric Field. Experiment 3.2: Paper Electrophoresis. Experiment 3.3: Charge Transport in Electrolyte Solution. Experiment 3.4: Conductance Titration. Experiment 3.5: Chemical Constitution and Electrolytic Conductance. Experiment 3.6: Faraday's Law. Experiment 3.7: Kinetics of Ester Saponification. Experiment 3.8: Movement of Ions and Hittorf Transport Number. Experiment 3.9: Polarographic Investigation of the Electroreduction of Formaldehyde. Experiment 3.10: Galvanostatic Measurement. Experiment 3.11: Cyclic Voltammetry. Experiment 3.12: Slow Scan Cyclic Voltammetry. Experiment 3.13: Kinetic Investigations with Cyclic Voltammetry. Experiment 3.14: Numerical Simulation of Cyclic Voltammograms. Experiment 3.15: Cyclic Voltammetry with Microelectrodes. Experiment 3.16: Cyclic Voltammetry of Organic Molecules. Experiment 3.17: Cyclic Voltammetry in Nonaqueous Solutions. Experiment 3.18: Cyclic Voltammetry with Sequential Electrode Processes. Experiment 3.19: Cyclic Voltammetry of Aromatic Hydrocarbons. Experiment 3.20: Cyclic Voltammetry of Aniline and Polyaniline. Experiment 3.21: Galvanostatic Step Measurements. Experiment 3.22: Chronoamperometry. Experiment 3.23: Chronocoulometry. Experiment 3.24: Rotating Disc Electrode. Experiment 3.25: Rotating Ring-Disc Electrode. Experiment 3.26: Measurement of Electrode Impedances. Experiment 3.27: Corrosion Cells. Experiment 3.28: Aeration Cell. Experiment 3.29 Concentration Cell. Experiment 3.30 Salt Water Drop Experiment According to Evans. Experiment 3.31: Passivation and Activation of an Iron Surface. Experiment 3.32: Cyclic Voltammetry with Corroding Electrodes. Experiment 3.33: Oscillating Reactions. 4 Analytical Electrochemistry. Experiment 4.1: Ion-sensitive Electrode. Experiment 4.2 Potentiometrically Indicated Titrations. Experiment 4.3 Bipotentiometrically Indicated Titration. Experiment 4.4 Conductometrically Indicated Titration. Experiment 4.5 Electrogravimetry. Experiment 4.6 Coulometric Titration. Experiment 4.7 Amperometry. Experiment 4.8 Polarography (Fundamentals). Experiment 4.9 Polarography (Advanced Methods). Experiment 4.10 Anodic Stripping Voltammetry. Experiment 4.11 Abrasive Stripping Voltammetry. Experiment 4.12 Polarographic Analysis of Anions. Experiment 4.13 Tensammetry. 5 Non-Traditional Electrochemistry. Experiment 5.1 UV-Vis Spectroscopy. Experiment 5.2 Surface Enhanced Raman Spectroscopy. Experiment 5.3 Infrared Spectroelectrochemistry. Experiment 5.4 Electrochromism. 6 Electrochemical Energy Conversion and Storage. Experiment 6.1 Lead Acid Accumulator. Experiment 6.2 Discharge Behavior of Nickel-Cadmium Accumulators. Experiment 6.3 Performance Data of a Fuel Cell. 7 Electrochemical Production. Experiment 7.1 Cementation Reaction. Experiment 7.2 Galvanic Copper Deposition. Experiment 7.3 Electrochemical Oxidation of Aluminum. Experiment 7.4 Kolbe Electrolysis of Acetic Acid. Experiment 7.5 Electrolysis of Acetyl Acetone. Experiment 7.6 Anodic Oxidation of Malonic Acid Diethylester. Experiment 7.7 Indirect Anodic Dimerization of Acetoacetic Ester (3-oxo-butyric acid ethyl ester). Experiment 7.8 Electrochemical Bromination of Acetone. Experiment 7.9 Electrochemical Iodination of Ethano. Experiment 7.10 Electrochemical Production. Experiment 7.11 Yield of Chlor-alkali Electrolysis According to the Diaphragm Process. Appendix. Index. |
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