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Fortschritte der Chemie Organischer Naturstoffe = Progress in the chemistry of organic natural products = Progres dans la chimie des substances organiques naturelles. Zehnter Band, tenth volume, Dixième volume

Author: K AlderJ AsselineauA ChatterjeeL FeinsteinM JacobsonAll authors
Publisher: Vienna : Springer Vienna, 1953.
Series: Fortschritte der Chemie Organischer Naturstoffe / Progress in the Chemistry of Organic Natural Products / Progres dans La Chimie des Substances Organiques Naturelles, 10.
Edition/Format:   eBook : Document : EnglishView all editions and formats
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Genre/Form: Electronic books
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: K Alder; J Asselineau; A Chatterjee; L Feinstein; M Jacobson; E Lederer; H Mark; G Rosenkranz; M Schumacher; F Sondheimer; L Zechmeister
ISBN: 9783709180037 3709180031
OCLC Number: 868136402
Description: 1 online resource.
Contents: - Contents - Table des matieres.- Anwendungen der Dien-Synthese fur die Erforschung von Naturstoffen.- A. Allgemeiner Teil.- I. Die philodiene Komponente.- II. Die Dien-Komponente.- 1. Diene.- 2. Die Tri- und Poly-ene.- 3. Die En-Synthese (indirekte substituierende Addition).- III. Der Retro-Dien-Zerfall.- IV. Die Dien-Synthese als stereochemisches Phanomen.- 1. Dien-Synthese und freie Drehbarkeit.- 2. Die sterischen Auswahlgesetze.- V. Dien-Synthesen mit unsymmetrischen Addenden.- VI. Dien-Synthese und Katalyse. Addition unter Bestrahlung. Anomalien in der Betatigung philodiener Funktionen. Glutardialdehyd als Ausgangsmaterial zur Synthese von achtgliedrigen Ringen.- B. Anwendungen.- VII. Synthetische Versuche zur Darstellung von Aldehyden des Cyclocitral- und Safranal-typus.- Verhalten hochmethylierter Butadiene bei Dien-Synthesen.- VIII. Dien-Synthesen zum. Nachweis von konjugierten Doppelbindungssystemen (Thebain, Muscarufin, Spilanthol).- IX. Dien-Synthesen in der Reihe der Fettsauren.- 1. Dienometrie.- 2. Saure von Mangold.- 3. ?- und ?-Elaostearinsaure.- 4. En-Synthesen mit Olsaure-methylester.- 5. Kombinierte En- und Dien-Synthesen mit Linol- und Linolensaure.- X. Dien-Synthesen in der Terpen-reihe.- 1. Acyclische Terpene (Myrten und Allo-ocirnen).- 2. Analyse und Genese der Pyronene.- 3. Dien-Synthesen mit Menthadienen.- 4. Neue Wege in die Reihe des m- und des p-Menthans.- 5. Bicyclische Terpene.- a) Nor-bornylan, Nor-borneol, Nor-campher.- b) Synthesen von naturlichen bicyclischen Terpenen.- c) Konfiguration der Campheralkohole.- d) Verallgemeinerung, Ausblick.- 6. Di-trpene.- XI. Steroide.- 1. Charakterisierung von Ergosterin und seinen Isomeren.- 2. Fraktionierte Dien-Synthesen. Vitamin D2 und Tachysterin.- 3. Darstellung oestrogener Carbonsauren. Beitrage zur Konfiguration von Equilenin und Oestron.- 4. Dien-Synthesen als Ausgangspunkt fur Totalsynthesen von Steroiden.- XII. Cantharidin-Synthese; das Cafestol.- XIII. Dien- und En-Synthesen mit molekularem Sauerstoff.- Ascaridol-Synthese. Zur Frage der Entstehung von aromatischen Kernen in Naturprodukten.- XIV. Bedient sich die Natur der Dien-Synthese als Aufbauprinzip?.- Physical Chemistry of Rubbers.- I. Introduction.- II. Fundamental Aspects of Rubberiness.- III. Structure and Molecular Weight of Rubbery Polymers.- A. Natural Rubber.- B. Synthetic Polyhydrocarbon Elastomers.- 1. Polyisobutylene and its Copolymers.- 2. Polybutadiene and Polyisoprene.- 3. Polychloroprene.- 4. Butadiene-Styrene Copolymers.- 5. Butadiene-Acrylonitrile Copolymers.- 6. Synthetic Elastomers of Various Other Types.- a) Rubber Elastic Polyesters and Polyamides.- b) Elastic Polyalkyl-siloxanes.- c) Other Synthetic Elastomers.- IV. Rubbery Materials in the Condensed State.- A. Crystallization of Polymers.- a) Natural Rubber.- b) Polychloroprene.- c) Polybutadiene and Polyisoprene.- d) Polyisobutylene.- e) Other Rubbery Polymers.- B. Transition Phenomena in Amorphous Polymers.- C. Crosslinked Amorphous Chain Networks.- V. Kinetic Theory of Rubber Elasticity.- A. Outline of the Theory.- B. Comparison with the Experiment.- References.- Chimie des lipides bacteriens.- I. Proprietes generales des lipides bacteriens.- II. Variations de la composition des lipides bacillaires.- Premiere Partie. Chimie des constituants des lipides bacteriens.- I. Substances hydroxylees.- a) Octadecanol et eicosanol.- b) ?-et ?-Leprosols.- c) Phtiocerol et substances apparentees.- II. Acides gras ramifies.- a) Acide (+) methyl-6 octanoique.- b) Acide tuberculostearique.- c) Acide lactobacillique.- d) Acide phytomonique.- e) Acides phtioiques: acides phtienoiques et acide mycolipenique-I.- f) Acide coryno-mycolique.- g) Acide coryno-mycolenique.- h) Corynine.- i) Acides mycoliques des Mycobacteries.- 1. Constitution chimique de l'acide ?-mycolique Test.- 2. Acides ?-, ?-et ?-mycoliques Test.- 3. Inventaire des acides mycoliques.- A. Acides mycoliques de souches humaines 208. - B. Acides mycoliques de souches bovines 211. - C. Acides mycoliques de M. phlei 212. - D. Acides mycoliques de M. smegmatis 212..- III. Biosynthese des acides gras des Bacteries.- Biosynthese des acides normaux.- Biosynthese des acides ramifies.- IV. Pigments lipo-solubles.- 1. Carotenoides.- a) Carotenoides specifiques des Bacteries.- 1. Leprotene 218. - 2. Rhodoviolascine 219. - 3. Rhodopine 219. - 4. Rhodovibrine 219. - 5. Rhodopurpurine 220. - 6. Flavorhodine 220. - 7. Sarcinine et sarcinaxanthine 220. - 8. Bacterioruberines ? et ? 220..- b) Les carotenoides de diverses especes de Bacteries.- 1. Mycobacteries 221. - 2. Corynebacteries 221. - 3. Actinomycetes 221. - 4. Rhodobacilles photosynthetiques 222. - 5. Staphylocoques 222. - 6. Streptocoques 222. - 7. Micrococcus 223..- c) Biosynthese des carotenoides des Bacteries.- 2. Naphtoquinones des Bacteries.- a) Vitamine K2.- b) Homologue superieur de la vitamine K2.- c) Phtiocol.- d) Role biologique des naphtoquinones des Bacteries.- Deuxieme Partie. Composition chimique des lipides bacillaires.- 1. Mycobacteries.- a) Graisses solubles dans l'acetone.- b) Phosphatides.- c) Cires A.- d) Cires B.- e) Cires C.- f) Cires D.- g) Autres preparations de lipo-polysaccharides complexes, isolees de Mycobacteries.- h) Lipides fortement lies.- i) Acides gras des diverses fractions lipidiques.- j) Comparaison de la composition des lipides de differentes souches de Mycobacteries.- k) Acido-resistance.- 2. Corynebacterium diphtheriae.- 3. Lactobacillus acidophilus et L. arabinosus.- 4. Phytomonas tumefaciens.- 5. Bacilles du genre Bacillus.- 6. Brucella.- 7. Escherichia.- 8. Malleomyces rnallei.- 9. Neisseria gonorrhoeae.- 10. Bacilles appartenant au genre Pseudomonas.- 11. Bacilles appartenant au genre Salmonella.- 12. Azotobacter chroococcum.- 13. Bacilles divers.- 14. Endotoxines.- 15. Membranes cellulaires.- Troisieme Partie. Proprietes biologiques des lipides bacillaires.- Bibliographie.- Syntheses of Cortisone.- I. Syntheses of Cortisone from Bile Acids.- 1. Conversion of Cholic to Desoxycholic Acid.- 2. Side-Chain Degradation.- 3. Introduction of Oxygen at C(11).- a) From a ?11-Ethylene by Addition of Hypobromous Acid (Reichstein).- b) From a C(12) Ketone by Removal of the C(12) Oxygen Group from an Intermediate 11,12-Ketol (Gallagher).- c) From a ?11-Ethylene or from a C(12) Ketone by Addition of Halogen to an Intermediate ?11-3 ?,9 ?-Oxide (Kendall).- d) From a ?9(11)-Ethylene by Oxidation of the 9 ?, II ?-Oxido-3?-01 to a 3?,9?-Oxido-3 ?-01-11-one (Heymann and Fieser).- e) From a ?9 (11)-Ethylene by Oxidation with Potassium Permanganate (Sarett; Wallis).- f) From a ?7, 9(11)-Dien (Fieser; Heusser and Jeger; Djerassi and Rosenkranz).- 4. Formation of the Dihydroxyacetone Side-chain and Introduction of the ?4-3-Ketone Function.- a) Method Involving Fischer Rearrangement of a Dihydroxy-aldehyde (Reichstein).- b) Method Involving Chromium Trioxide Oxidation of a 17 ?,20,21-triol 21-Acetate (Sarett).- c) Method Involving Simultaneous Hydroxylation and Oxidation of a ?17(20)-21-01 Acetate (Miescher).- d) Method Involving Hydroxylation of a?17(20)-20-Cyano-21-01 Acetate (Sarett).- e) Method Involving Hydroxylation of a?17(20)-20-Bromo-21-01 Acetate (Wagner and Moore).- f) Method Involving Reduction of the Oxide of a ?16-20-One-21-01 Acetate (Kendall).- g) Methods for Introducing the ?4-Double Bond into 4,5 ?-Dihydrocortisone Acetate (Kendall).- h) Methods Involving the Introduction of the 17?-Hydroxyl Group Prior to that at C(21) (Sarett; Gallagher).- II. Syntheses of Cortisone from Steroids with Ring C Unsubstituted.- 1. Introduction of Oxygen at C(11) and Side-chain Degradation.- a) Method Involving Hydration of a ?7-9 ?,11 ?-Oxide (Tishler; Heusser and Jeger).- b) Method Involving Oxidation of a ?7, 9(11)-Diene with Sodium Dichromate (Fieser).- c) Method Involving Interaction of a ?7, 9(11)-Dien with N-Bromosuccinimide (Fieser).- d) Method Involving Oxidation of a ?7, 9(11)-Dien with Performic Acid (Stork, Rosenkranz and Djerassi).- e) Utilization of ?8-7-Ketones (Djerassi and Rosenkranz).- f) Method Involving Chemical Reduction of a?8-11-One (Sondheimer, Djerassi and Rosenkranz; Tishler).- 2. Formation of the Dihydroxyacetone Side-chain and Introduction of the ?4-3-Ketone Function.- III. Synthesis of Cortisone from Sarmentogenin.- IV. Synthesis of Cortisone from Hecogenin.- V. Total Syntheses of Cortisone.- 1. Synthesis According to Robinson and Cornforth.- 2. Synthesis According to Woodward, Sondheimer and Taub.- 3. Alternative Synthesis Investigated by Robinson.- 4. Synthesis According to Sarett.- VI. Biochemical Syntheses of Cortisone.- 1. Oxygenation by Means of Adrenal Glands.- 2. Microbiological Oxygenation.- VII. Syntheses of 17?-Hydroxy-corticosterone.- References.- Addendum.- Rauwolfia Alkaloids.- I. Introduction.- II. The Alkaloid of Rauwolfia canescens.- Rauwolscine.- The Pharmacology of Rauwolscine.- III. The Alkaloids of Rauwolfia serpentina.- Ajmaline.- Ajmalinine.- Ajmalicine.- Serpentinine.- Serpentine.- Reserpine.- Rauwolfinine.- The Pharmacology of Rauwolfia serpentine.- Pharmacology of Reserpine.- IV. The Alkaloids of Rauwolfia vomitoria and R. obscura.- Alstonine.- The Pharmacology of Rauwolfia vomitoria and R. obscura.- V. The Alkaloids of Further Rauwolfia Species.- Rauwolfia caffra.- The Pharmacology of Rauwolfine.- Rauwolfia heterophylla.- The Pharmacology of R. heterophylla.- Rauwolfia natalensis.- Rauwolfia mombasiana.- VI. Conclusions.- References.- Insecticides Occurring in Higher Plants.- I. Introduction.- II. Nicotine and other Tobacco Alkaloids.- 1. General Remarks.- 2. Origin of Nicotine, Anabasine and Nornicotine.- 3. Insecticidal Use.- 4. Analysis.- 5. Toxicity.- III. Rotenone and Related Compounds.- 1. General Remarks.- 2. Chemical Structure.- A. Rotenone.- B. Deguelin.- C. Tephrosin.- D. Toxicarol.- E. Sumatrol.- F. Malaccol.- G. Elliptone.- 3. Insecticidal Action.- 4. Pharmacology.- IV. Pyrethrum.- 1. General Remarks.- 2. Chemical Structure.- 3. Toxicity and Pharmacology.- 4. Synthetic Products.- V. Unsaturated Isobutylamides.- 1. Pellitorine.- 2. Spilanthol.- 3. Affinin.- 4. Herculin.- 5. Sanshool-I and Sanshool-II.- 6. Scabrin.- VI. Synergetic Effects.- 1. Sesamin and Related Compounds.- 2. Piperine.- VII. Essential Oils, Camphor, Turpentine, Fatty Oils.- VIII. Miscellaneous.- 1. Ryania speciosa.- 2. Tripterygium wilfordii Hoox.- 3. Quassia.- 4. Sabadilla.- 5. Hellebore (Veratrum).- 6. Larkspur.- 7. Mamey.- References.- Namenverzeichnis. Index of Names. Index des Auteurs.- Sachverzeichnis. Index of Subjects. Index des Matieres.
Series Title: Fortschritte der Chemie Organischer Naturstoffe / Progress in the Chemistry of Organic Natural Products / Progres dans La Chimie des Substances Organiques Naturelles, 10.
Other Titles: Progress in the chemistry of organic natural products
Progres dans la chimie des substances organiques naturelles
Responsibility: herausgegeben von, edited by, rédigé par L. Zechmeister, California Institute of Technology, Pasadena ; K. Alder, J. Asselineuz, A. Chatterjee, L. Feinstein, M. Jacobson, E. Lederer, H. Mark, G. Rosenkranz, M. Schumacher, F. Sondheimer.

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