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| Document Type: | Book |
|---|---|
| All Authors / Contributors: |
Brian C Smith |
| ISBN: | 9781420069297 1420069292 |
| OCLC Number: | 166358484 |
| Description: | xiii, 193 p. : ill. ; 25 cm. |
| Contents: | Machine generated contents note: ch. 1 Introduction to Infrared Spectroscopy -- I. Terms and Definitions -- II. The Properties of Light -- III. What Is an Infrared Spectrum? -- IV. What Are Infrared Spectra Used For? -- V. The Advantages and Disadvantages of Infrared Spectroscopy -- VI. The Advantages and Disadvantages of FTIR -- A. The Advantages of FTIRs -- B. The Disadvantage of FTIR -- VII. FTIR: The Rest of the Story -- References -- ch. 2 How an FTIR Works -- I. Interferometers and Interferograms -- A. How Many Scans Should Be Used? -- II. How an Interferogram Becomes a Spectrum -- A. Scanning Advice -- III. Instrumental Resolution -- A. What Determines Resolution in an FTIR Scan? -- B. What Resolution Should Be Used? -- IV. FTIR Trading Rules -- V. FTIR Hardware -- A. Interferometers -- B. Infrared Sources -- C. Beamsplitters -- D. Infrared Detectors -- E. The Laser -- VI. Testing Instrument Quality and Troubleshooting -- References -- ch. 3 Proper Use of Spectral Processing I. The Rules of Spectral Processing -- II. Spectral Subtraction -- A. Subtraction Artifacts -- III. Baseline Correction -- IV. Smoothing -- V. Spectral Derivatives -- VI. Deconvolution -- A. Guidance, Precautions, and Limitations -- VII. Spectral Library Searching -- A. The Search Process -- B. Interpreting Library Search Results -- VIII. Analysis of Mixtures: Subtract and Search Again -- References -- ch. 4 Preparing Samples Properly -- I. Transmission Sampling Overview -- A. Windows, Cells, and Materials for Transmission Analysis -- II. Transmission Analysis of Solids and Powders -- A. KBr Pellets -- 1. Mechanical Grinding -- 2. Advantages and Disadvantages of KBr Pellets -- B. Mulls -- 1. The Split Mull Method -- III. Transmission Analysis of Polymers -- A. The Cast Film Method -- B. The Heat and Pressure Method -- IV. Transmission Analysis of Liquids -- A. Capillary Thin Films -- B. Sealed Liquid Cells -- V. Transmission Analysis of Gases and Vapors -- VI. Reflectance Analysis -- A. Different Types of Reflectance -- B. Advantages and Disadvantages of Reflectance Sampling VII. Specular Reflectance -- VIII. Diffuse Reflectance (DRIFTS) -- A. Abrasive Sampling -- IX. Attenuated Total Reflectance (ATR) -- A. Depth of Penetration -- X. Applications of ATR -- A. Liquids -- B. Semi-Solids -- C. Polymers -- D. Powders -- XI. ATR: Advantages and Disadvantages -- XII. FTIR Sample Preparation: Overview and Recommendations -- References -- ch. 5 Quantitative Infrared Spectroscopy -- I. Terms and Definitions -- II. Beer's Law -- III. Calibration and Prediction with Beer's Law -- A. Calibration -- B. Prediction -- C. An Experimental Protocol for Single Component Analyses -- 1. Analyzing for a Single Analyte -- IV. Measuring Absorbances Properly -- A. Peak Areas versus Peak Heights -- B. Dealing with Overlapped Peaks -- V. Avoiding Experimental Errors -- References -- ch. 6 Infrared Microscopy -- I. Hyphenated Infrared Techniques -- II. Infrared Microscopy Instrumentation -- III. Sample Preparation -- IV. Applications -- V. Infrared Mapping and Imaging -- References. |
| Responsibility: | Brian C. Smith. |
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Related Subjects:(3)
- Fourier transform infrared spectroscopy.
- Fourier, Transformations de.
- Fourier, Spectroscopie infrarouge à transformée de.
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