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Gas chromatography and mass spectrometry : a practical guide

Author: O David Sparkman; Zelda Penton; Fulton G Kitson
Publisher: Amsterdam ; San Diego : Elsevier/Academic Press, ©2011.
Edition/Format:   Print book : English : 2nd edView all editions and formats
Summary:

Covers the practical instruction necessary for successful operation of GC/MS equipment. This title reviews the advances in instrumentation, ionization methods, and quantitation. It includes  Read more...

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Document Type: Book
All Authors / Contributors: O David Sparkman; Zelda Penton; Fulton G Kitson
ISBN: 9780123736284 0123736285
OCLC Number: 777776894
Description: xix, 611 pages : illustrations ; 23 cm
Contents: The fundamentals of GC/MS --
Introduction and history --
Gas chromatography --
The gc/ms interface --
Mass spectrometry instrumentation --
Mass spectral data interpretation --
Quantitation with GC/MS --
GC conditions, derivatization, and mass spectral interpretation --
Of specific compound types --
Acids --
Alcohols --
Aldehydes --
Amides --
Amines --
Amino acid --
Common contaminants --
Drugs and their metabolites --
Esters --
Ethers --
Fluorinated compounds --
Gases --
Glycols --
Halogenated compounds (other than fluorinated) --
Hydrocarbons --
Isocyanates --
Ketones --
Nitriles --
Nitroaromatics --
Nitrogen-containing heterocyclics --
Nucleosides (TMS derivatives) --
Pesticides --
Phenols --
Phosphorus compounds --
Plasticizers and other polymer additives (including phthalates) --
Prostaglandins (MO-TMS derivatives) --
Solvents and their impurities --
Steroids --
Sugars (monosaccharides) --
Sulfur compounds --
Appendices --
A definitions of terms related to gas chromatography --
B definitions of terms related to mass spectrometry --
C atomic masses and isotope abundances --
X+1 and x+2 values for ions containing atoms of C and H based on --
Isotope contributions --
E isotope peak patterns for ions containing atoms of Cl and/or Br --
F steps to follow in the determination of an elemental composition --
Based on isotope peak intensity ratios --
G derivatization in GC/MS --
H points of comparison of LC/MS vs GC/MS --
I list of available EI mass spectral databases --
J information required for reporting a GC/MS analysis --
K third-party software for use with GC/MS --
GC installation and maintenance --
Troubleshooting common GC problems --
N maintenance, operating tips, and troubleshooting for mass spectrometers --
O mixtures for determining mass spectral resolution --
P cross-index chart for GC stationary phases --
Q ions for determining unknown structures.
Responsibility: O. David Sparkman, Zelda E. Penton, Fulton G. Kitson.

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"The authors have kept this book relevant and timely and have achieved their goal of providing useful information for practitioners. They understand what those who actually use GC/MS need, and Read more...

 
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