skip to content
Laboratory experiments using microwave heating Preview this item
ClosePreview this item
Checking...

Laboratory experiments using microwave heating

Author: Nicholas E Leadbeater; Cynthia B McGowan
Publisher: Boca Raton : CRC Press, Taylor & Francis Group, 2013.
Edition/Format:   Print book : EnglishView all editions and formats
Database:WorldCat
Summary:
"This book presents a series of procedures for organic, inorganic, analytical, and physical chemistry experiments. Each experimental protocol comprises a chapter in the text that is available for purchase individually. Each protocol contains a brief introduction to the concepts behind the chemistry covered, followed by detailed procedures for performing the reaction using a small and a larger microwave unit. The  Read more...
Rating:

(not yet rated) 0 with reviews - Be the first.

Subjects
More like this

 

Find a copy in the library

&AllPage.SpinnerRetrieving; Finding libraries that hold this item...

Details

Genre/Form: Laboratory manuals
Document Type: Book
All Authors / Contributors: Nicholas E Leadbeater; Cynthia B McGowan
ISBN: 9781439856093 1439856095
OCLC Number: 826860908
Notes: Includes index.
Description: pages cm
Contents: Introduction: Using microwave heating in chemistry: the basics --
Experiment 1: Diels-Alder cycloaddition reaction --
Experiment 2: Second-order elimination reaction: preparation of heptene from 2-bromoheptane --
Experiment 3: An addition-elimination sequence preparation of a bromoalkene --
Experiment 4: Fischer esterification: preparation of ethyl-4-aminobenzoate (benzocaine) --
Experiment 5: Transesterification reaction: preparation of biodiesel --
Experiment 6: Knoevenagel condensation reaction: preparation of 3-acetylcoumarin --
Experiment 7: The Perkin reaction: condensation of an aromatic aldehyde with rhodanine --
Experiment 8: Williamson ether synthesis: preparation of allyl phenyl ether --
Experiment 9: Claisen rearrangement: preparation of 2-allyl phenol from allyl phenyl ether --
Experiment 10: Hydration of an alkyne: preparation of acetophenone from phenylacetylene --
Experiment 11: Oxidation of secondary alcohol: preparation of a ketone --
Experiment 12: Suzuki coupling reaction:preparation of a biaryl --
Experiment 13: Heck reaction: preparation of substituted cinnamic acids --
Experiment 14: Preparation of an aryl nitrile: application of a copper-catalyzed cyanation reaction --
Experiment 15: Alkene metathesis: preparation of a substituted cyclopentene --
Experiment 16: Click reaction: preparation of a triazole --
Experiment 17: Coordination chemistry: preparation of cisplatin --
Experiment 18: Preparation of a palladium complex: bis(triphenylphosphine)palladium(II) dichloride --
Experiment 19: Coordination of an aromatic ring to a metal: preparation of an arene chromium tricarbonyl complex --
Experiment 20: Determination of an empirical formula: zinc bromide --
Experiment 21: Microwave-assisted extraction: identification of the major flavor components of citrus oil --
Experiment 22: Microwave-assisted digestion of dietary supplements: metal analysis by atomic absorption spectroscopy.
Responsibility: Nicholas E. Leadbeater & Cynthia B. McGowan.
More information:

Abstract:

"This book presents a series of procedures for organic, inorganic, analytical, and physical chemistry experiments. Each experimental protocol comprises a chapter in the text that is available for purchase individually. Each protocol contains a brief introduction to the concepts behind the chemistry covered, followed by detailed procedures for performing the reaction using a small and a larger microwave unit. The book covers all commonly available scientific microwave apparatus currently used in teaching laboratories. Each chapter concludes with questions for students to answer as part of their laboratory write-up. The experiments are also featured online as well as on a complementary CD-ROM. The author maintains a website with supplemental information"--

Reviews

Editorial reviews

Publisher Synopsis

"The book starts with a short and easy-to-understand introduction to the basics of microwave heating, which in my opinion every microwave user should know. ... Designed as a textbook for the Read more...

 
User-contributed reviews
Retrieving GoodReads reviews...
Retrieving DOGObooks reviews...

Tags

Be the first.
Confirm this request

You may have already requested this item. Please select Ok if you would like to proceed with this request anyway.

Linked Data


Primary Entity

<http://www.worldcat.org/oclc/826860908> # Laboratory experiments using microwave heating
    a schema:CreativeWork, schema:Book ;
   library:oclcnum "826860908" ;
   library:placeOfPublication <http://id.loc.gov/vocabulary/countries/flu> ;
   schema:about <http://id.worldcat.org/fast/1020213> ; # Microwave heating
   schema:about <http://id.worldcat.org/fast/853344> ; # Chemistry
   schema:about <http://dewey.info/class/542.4/e23/> ;
   schema:about <http://id.worldcat.org/fast/1020270> ; # Microwaves--Industrial applications
   schema:about <http://id.worldcat.org/fast/853375> ; # Chemistry--Experiments
   schema:about <http://experiment.worldcat.org/entity/work/data/1083642863#Topic/science_chemistry_general> ; # SCIENCE--Chemistry--General
   schema:about <http://experiment.worldcat.org/entity/work/data/1083642863#Topic/science_chemistry_organic> ; # SCIENCE--Chemistry--Organic
   schema:about <http://experiment.worldcat.org/entity/work/data/1083642863#Topic/microwaves_industrial_applications> ; # Microwaves--Industrial applications
   schema:about <http://id.loc.gov/authorities/subjects/sh85022996> ; # Chemistry--Experiments
   schema:bookFormat bgn:PrintBook ;
   schema:contributor <http://experiment.worldcat.org/entity/work/data/1083642863#Person/mcgowan_cynthia_b> ; # Cynthia B. McGowan
   schema:creator <http://viaf.org/viaf/131589456> ; # Nicholas E. Leadbeater
   schema:datePublished "2013" ;
   schema:description "Introduction: Using microwave heating in chemistry: the basics -- Experiment 1: Diels-Alder cycloaddition reaction -- Experiment 2: Second-order elimination reaction: preparation of heptene from 2-bromoheptane -- Experiment 3: An addition-elimination sequence preparation of a bromoalkene -- Experiment 4: Fischer esterification: preparation of ethyl-4-aminobenzoate (benzocaine) -- Experiment 5: Transesterification reaction: preparation of biodiesel -- Experiment 6: Knoevenagel condensation reaction: preparation of 3-acetylcoumarin -- Experiment 7: The Perkin reaction: condensation of an aromatic aldehyde with rhodanine -- Experiment 8: Williamson ether synthesis: preparation of allyl phenyl ether -- Experiment 9: Claisen rearrangement: preparation of 2-allyl phenol from allyl phenyl ether -- Experiment 10: Hydration of an alkyne: preparation of acetophenone from phenylacetylene -- Experiment 11: Oxidation of secondary alcohol: preparation of a ketone -- Experiment 12: Suzuki coupling reaction:preparation of a biaryl -- Experiment 13: Heck reaction: preparation of substituted cinnamic acids -- Experiment 14: Preparation of an aryl nitrile: application of a copper-catalyzed cyanation reaction -- Experiment 15: Alkene metathesis: preparation of a substituted cyclopentene -- Experiment 16: Click reaction: preparation of a triazole -- Experiment 17: Coordination chemistry: preparation of cisplatin -- Experiment 18: Preparation of a palladium complex: bis(triphenylphosphine)palladium(II) dichloride -- Experiment 19: Coordination of an aromatic ring to a metal: preparation of an arene chromium tricarbonyl complex -- Experiment 20: Determination of an empirical formula: zinc bromide -- Experiment 21: Microwave-assisted extraction: identification of the major flavor components of citrus oil -- Experiment 22: Microwave-assisted digestion of dietary supplements: metal analysis by atomic absorption spectroscopy."@en ;
   schema:description ""This book presents a series of procedures for organic, inorganic, analytical, and physical chemistry experiments. Each experimental protocol comprises a chapter in the text that is available for purchase individually. Each protocol contains a brief introduction to the concepts behind the chemistry covered, followed by detailed procedures for performing the reaction using a small and a larger microwave unit. The book covers all commonly available scientific microwave apparatus currently used in teaching laboratories. Each chapter concludes with questions for students to answer as part of their laboratory write-up. The experiments are also featured online as well as on a complementary CD-ROM. The author maintains a website with supplemental information"--"@en ;
   schema:exampleOfWork <http://worldcat.org/entity/work/id/1083642863> ;
   schema:genre "Laboratory manuals"@en ;
   schema:inLanguage "en" ;
   schema:name "Laboratory experiments using microwave heating"@en ;
   schema:productID "826860908" ;
   schema:workExample <http://worldcat.org/isbn/9781439856093> ;
   wdrs:describedby <http://www.worldcat.org/title/-/oclc/826860908> ;
    .


Related Entities

<http://experiment.worldcat.org/entity/work/data/1083642863#Person/mcgowan_cynthia_b> # Cynthia B. McGowan
    a schema:Person ;
   schema:familyName "McGowan" ;
   schema:givenName "Cynthia B." ;
   schema:name "Cynthia B. McGowan" ;
    .

<http://experiment.worldcat.org/entity/work/data/1083642863#Topic/science_chemistry_general> # SCIENCE--Chemistry--General
    a schema:Intangible ;
   schema:name "SCIENCE--Chemistry--General"@en ;
    .

<http://experiment.worldcat.org/entity/work/data/1083642863#Topic/science_chemistry_organic> # SCIENCE--Chemistry--Organic
    a schema:Intangible ;
   schema:name "SCIENCE--Chemistry--Organic"@en ;
    .

<http://id.loc.gov/authorities/subjects/sh85022996> # Chemistry--Experiments
    a schema:Intangible ;
   schema:name "Chemistry--Experiments"@en ;
    .

<http://id.worldcat.org/fast/1020213> # Microwave heating
    a schema:Intangible ;
   schema:name "Microwave heating"@en ;
    .

<http://id.worldcat.org/fast/1020270> # Microwaves--Industrial applications
    a schema:Intangible ;
   schema:name "Microwaves--Industrial applications"@en ;
    .

<http://id.worldcat.org/fast/853344> # Chemistry
    a schema:Intangible ;
   schema:name "Chemistry"@en ;
    .

<http://id.worldcat.org/fast/853375> # Chemistry--Experiments
    a schema:Intangible ;
   schema:name "Chemistry--Experiments"@en ;
    .

<http://viaf.org/viaf/131589456> # Nicholas E. Leadbeater
    a schema:Person ;
   schema:familyName "Leadbeater" ;
   schema:givenName "Nicholas E." ;
   schema:name "Nicholas E. Leadbeater" ;
    .

<http://worldcat.org/isbn/9781439856093>
    a schema:ProductModel ;
   schema:isbn "1439856095" ;
   schema:isbn "9781439856093" ;
    .


Content-negotiable representations

Close Window

Please sign in to WorldCat 

Don't have an account? You can easily create a free account.