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Microreactors in preparative chemistry : practical aspects in bioprocessing, nanotechnology, catalysis and more

Author: Wladimir Reschetilowski
Publisher: Weinheim : Wiley-VCH, [2013]
Edition/Format:   Print book : EnglishView all editions and formats
Summary:
This is the first book in the field to focus on these aspects, providing extremely valuable information unavailable elsewhere for anyone seeking the practical application of microreactor technology in preparative chemistry. The topics covered branch out in three different directions. To begin with, the knowledge necessary for the preparative chemistry concerning the influence of the so-called microeffects on the  Read more...
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Genre/Form: Aufsatzsammlung
Material Type: Internet resource
Document Type: Book, Internet Resource
All Authors / Contributors: Wladimir Reschetilowski
ISBN: 9783527332823 3527332820 9789783527652 9783527657 9783527652914 3527652914 9783527652907 3527652906 9783527652891 3527652892 3527652922 9783527652921
OCLC Number: 847542514
Description: xv, 335 pages : illustrations ; 24 cm
Contents: PREFACE PRINCIPLES OF MICROPROCESS TECHNOLOGY Introduction History Basic Characteristics Industrial Applications Concluding Remarks EFFECTS OF MICROFLUIDICS ON PREPARATIVE CHEMISTRY PROCESSES Introduction Mixing Heat Management Mass Transfer and Chemical Reactions Flow Separation Numbering-Up Strategy Practical Exercise: Experimental Characterization of Mixing in Microstructured Reactors MODULAR MICRO- AND MILLIREACTOR SYSTEMS FOR PREPARATIVE CHEMICAL SYNTHESIS AND BIOPROCESSES Introduction Modular Microreaction System Examples for Microreactor Applications Laboratory Exercise: Suzuki Reaction in a Modular Microreactor Setup POTENTIAL OF LAB-ON-A-CHIP: SYNTHESIS, SEPARATION, AND ANALYSIS OF BIOMOLECULES Introduction Learning from Nature: Analogies to Living Cells Microenzyme Reactors Microchip Electrophoresis Microenzyme Membrane Reactor/Micromembrane Chromatography Nucleic Acid Analysis in Microchannels Saccharide Analyses in Microdevices Practical Exercise: Lipase-Catalyzed Esterification Reaction BIOPROCESSING IN MICROREACTORS Introduction Background Practical Exercise: Functionalization of Silicon Surface SYNTHESIS OF FINE CHEMICALS Introduction Organic Synthesis in Liquid and Liquid - Liquid Phases Gas - Liquid Biphasic Organic Synthesis Practical Exercise: Photochemical Generation of Singlet Oxygen and Its [4 + 2] Cycloaddition to Cyclopentadiene SYNTHESIS OF NANOMATERIALS USING CONTINUOUS-FLOW MICROREACTORS Introduction Microfluidic Devices Synthesis of Nanomaterials Using Microreactors Kinetic Studies Process Optimization Point-of-Use Synthesis and Deposition Practical Exercises: Synthesis of Nanocrystals POLYMERIZATION IN MICROFLUIDIC REACTORS Introduction Practical Considerations Single-Phase Polymerization Multiphase Polymerization Beyond Synthesis: New Developments for Next-Generation MF Polymerization Practical Exercise: MF Polymerization Reactor Kinetics Studies Using In Situ Characterization ELECTROCHEMICAL REACTIONS IN MICROREACTORS Introduction Electrode Configuration Electrolysis without Supporting Electrolytes Generation and Reactions with Unstable Intermediates Practical Exercise: Electrochemical Reactions in Flow Microreactors HETEROGENEOUS CATALYSIS IN MICROREACTORS Introduction Bulk Catalysts Supported Catalysts Mesoporous Supports Microporous Supports Practical Exercise: PdZn/TiO2-Catalyzed Selective Hydrogenation of Acetylene Alcohols in a Capillary Microreactor CHEMICAL INTENSIFICATION IN FLOW CHEMISTRY THROUGH HARSH REACTION CONDITIONS AND NEW REACTION DESIGN Introduction High-Temperature Processing in Microflow High-Pressure Processing in Microflow Solvent Effects in Microflow Ex-Regime Processing and Handling of Hazardous Compounds in Microflow New Chemical Transformations in Microflow Process Integration in Microflow Practical Exercises MODELING IN MICROREACTORS Introduction Processes in Microreactors and the Role of Mixing Modeling of Processes in Microreactors Based on General Balance Equation Computation of Reaction Flows in Microreactors Practical Exercise: Alkylation of Phenylacetonitrile INDEX
Responsibility: edited by Wladimir Reschetilowski.

Abstract:

This is the first book in the field to focus on these aspects, providing extremely valuable information unavailable elsewhere for anyone seeking the practical application of microreactor technology  Read more...

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