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Microwave-assisted sample preparation for trace element determination

Author: Érico Marlon Moraes Flores
Publisher: Amsterdam : Elsevier, 2014.
Edition/Format:   eBook : Document : EnglishView all editions and formats
Summary:
Microwave-Assisted Sample Preparation for Trace Element Analysis describes the principles, equipment, and applications involved in sample preparation with microwaves for trace element analysis. The book covers well-established applications as well as new trends in this field. Hot topics such as sample preparation for speciation, metabolomics, and halogen determination, as well as the alternatives of sample  Read more...
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Genre/Form: Electronic books
Additional Physical Format: Print version:
Microwave-assisted sample preparation for trace element analysis.
Amsterdam : Elsevier, 2013
(OCoLC)857524325
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: Érico Marlon Moraes Flores
ISBN: 9780444594440 0444594442
OCLC Number: 885408692
Notes: "Microwave-assisted sample preparation for trace element analysis"--Ebook main page, titile.
Description: 1 online resource (xiv, 400 pages) : illustrations
Contents: Front Cover; Microwave-Assisted Sample Preparation for Trace Element Determination; Copyright; Contents; Preface; List of Contributors; Chapter 1 --
Introduction to Sample Preparation for Trace Element Determination; 1.1. INTRODUCTION; 1.2. THE ANALYTICAL SEQUENCE; 1.3. ANALYTICAL EFFICIENCY AND ROBUSTNESS; 1.4. SYSTEMATIC ERRORS IN SAMPLE PREPARATION; 1.5. PRELIMINARY PROCESSES, TREATMENTS; 1.6. COMMENTS ON CONVENTIONAL OPEN AND CLOSED SYSTEMS FOR SAMPLE PREPARATION; 1.7. CONCLUSION; REFERENCES; Chapter 2 --
Microwave Heating; 2.1. INTRODUCTION. 2.2. GENERAL ASPECTS OF ENERGY AND MATTER INTERACTION2.3. DIELECTRIC HEATING; 2.4. ADDITIONAL ASPECTS TO CONSIDER IN MICROWAVE HEATING; 2.5. MICROWAVE HEATING IN SAMPLE PREPARATION; 2.6. FINAL REMARKS; REFERENCES; Chapter 3 --
Systems for Microwave-Assisted Wet Digestion; 3.1. INTRODUCTION; 3.2. OPEN SYSTEMS; 3.3. CLOSED SYSTEMS; 3.4. HISTORY OF MICROWAVE SYSTEMS AND CURRENT TECHNOLOGY; 3.5. FLOW SYSTEMS; 3.6. FINAL REMARKS AND FUTURE TRENDS; REFERENCES; Chapter 4 --
Wet Digestion Using Microwave Heating; 4.1. MICROWAVE-ASSISTED WET SAMPLE DIGESTION. 4.2. DEVELOPMENT AND EVALUATION OF MICROWAVE-ASSISTED WET DIGESTION PROCEDURES4.3. APPLICATIONS OF MICROWAVE-ASSISTED PROCEDURES FOR SAMPLE DIGESTION; REFERENCES; Chapter 5 --
Microwave-Induced Combustion; 5.1. INTRODUCTION; 5.2. COMBUSTION SYSTEMS FOR SAMPLE DIGESTION; 5.3. APPARATUS AND PROCEDURES FOR MIC; 5.4. FOCUSED MICROWAVE-INDUCED COMBUSTION; 5.5. ABSORBING SOLUTIONS; 5.6. ALTERNATIVE USES OF MIC; 5.7. FINAL REMARKS; REFERENCES; Chapter 6 --
Diluted Acids in Microwave-Assisted Wet Digestion; 6.1. INTRODUCTION; 6.2. DILUTED ACIDS IN MICROWAVE-ASSISTED WET DIGESTION IN CLOSED VESSELS. 6.3. OTHER STRATEGIES TO REDUCE THE AMOUNTS OF ACIDS FOR DIGESTION6.4. FINAL REMARKS; REFERENCES; Chapter 7 --
Microwave-Assisted Ultraviolet Digestion; 7.1. INTRODUCTION; 7.2. MW-UV METHOD; 7.3. COMMERCIAL SYSTEMS FOR MW-UV; 7.4. APPLICATIONS IN CHEMISTRY; 7.5. FINAL CONSIDERATIONS; REFERENCES; Chapter 8 --
Microwave-Assisted Extraction; 8.1. INTRODUCTION; 8.2. PRINCIPLES AND TECHNOLOGIES; 8.3. CURRENT APPLICATIONS; REFERENCES; Chapter 9 --
Flow Digestion Systems with Microwave and Conductive Heating; 9.1. SYSTEMATIC ERRORS IN SAMPLE DIGESTION: GENERAL ASPECTS RELATED TO FLOW DIGESTION. 9.2. DELETERIOUS EFFECTS OF CARBON IN ICP-BASED ELEMENTAL ANALYSIS9.3. PRINCIPLES OF FLOW DIGESTION SYSTEMS; 9.4. FLOW DIGESTION AT AMBIENT PRESSURE; 9.5. FLOW DIGESTION AT MEDIUM PRESSURE; 9.6. HIGH-PRESSURE FLOW DIGESTION SYSTEMS; 9.7. COMPONENTS OF FLOW DIGESTION SYSTEMS; 9.8. STRUCTURAL MATERIALS AND DISSOLUTION REAGENTS FOR FLOW DIGESTION SYSTEMS; 9.9. FLOW DIGESTION OF SLURRIES; REFERENCES; Chapter 10 --
Microwave-Assisted Sample Preparation for Element Speciation; 10.1. INTRODUCTION; 10.2. MERCURY SPECIATION; 10.3. ORGANOTIN SPECIATION; 10.4. SELENIUM SPECIATION.
Responsibility: edited by Érico Marlon Moraes Flores.

Abstract:

Describes the principles, equipment, and applications involved in sample preparation with microwaves for trace element analysis. This book covers applications as well as fresh trends in this field.  Read more...

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