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Organic syntheses, collective volume 6 : a revised edition of annual volumes 50-59

Author: Wayland E Noland
Publisher: New York : Wiley, ©1988.
Edition/Format:   Print book : EnglishView all editions and formats
Database:WorldCat
Summary:

This volume contains the procedures previously published in annual volumes 50-59, revised and updated where necessary. Efforts have been made to standardize the style of experimental procedures and  Read more...

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Document Type: Book
All Authors / Contributors: Wayland E Noland
ISBN: 0471852430 9780471852438
OCLC Number: 16567487
Notes: Text on front end-papers.
Includes indexes.
Description: xviii, 1208 pages : illustrations, portrait ; 24 cm
Contents: [The numbers in parentheses refer to the annual volume (in boldface type) and page number where each procedure first appeared] Acylamidoalkyl Acetophenones from Substituted Phenethylamines: 2-(2-Acetamidoethyl)-4,5-dimethoxyacetophenone (56, 3) Thiol Protection with the Acetamidomethyl Group: S-Acetamidomethyl-l-cysteine Hydrochloride (59, 190) Acetic Formic Anhydride (50, 1) Acetone Hydrazone (50, 3) Preparation of Hydrazones: Acetophenone Hydrazone (50, 102) 3beta-Acetoxy-5alpha-cyanocholestan-7-one (52, 100) p-Acetyl-alpha-bromohydrocinnamic Acid (51, 1) alpha,beta-Dehydrogenation of beta-Dicarbonyl Compounds by Selenoxide Elimination: 2-Acetyl-2-cyclohexen-1-one (59, 58) 2-Acetyl-1,3-cyclopentanedione (52, 1) 3-Acetyl-2,4-dimethylfuran (53, 1) 2-Acetyl-6-methoxynaphthalene (53, 5) Copper Catalyzed Arylation of beta-Dicarbonyl Compounds: 2-(1-Acetyl-2-oxopropyl)benzoic Acid (58, 52) 5-Acetyl- 1,2,3,4,5-pentamethylcyclopentadiene (56, 1) 2-Adamantanecarbonitrile (57, 8) Tertiary Alcohols from Hydrocarbons by Ozonation on Silica Gel: 1-Adamantanol (59, 176) Adamantanone (53, 8) Enone Reduction-Enolate Alkylation Sequence: 2-Allyl-3-methylcyclohexanone (56, 52) Preparation of N-Aminoaziridines: trans-1-Amino-2,3-diphenylaziridine, 1-Amino-2-phenylaziridine, and 1-Amino-2-phenylaziridinium Acetate (55, 114) Reduction of Ketones by Use of the Tosylhydrazone Derivatives: Androstan-17beta-Ol (52, 122) Aldehydes from 4,4-Dimethyl-2-oxazoline and Grignard Reagents: o-Anisaldehyde (54, 42) [18]Annulene (54, 1) Azetidine (53, 13) Azoethane (52, 11) Diels-Alder Addition of Perchlorobenzyne: Benzobarrelene (59, 71) Benzocyclopropene (55, 12) alpha-Chlorination of Carboxylic Acids Mediated by Chlorosulfonic Acid: Phis-Benzoylamino-alpha-chlorocaproic Acid (59, 20) 1-N-Acylamino-1,3-dienes from 2,4-pentadienoic Acids by the Curtius Rearrangement: Benzyl trans-1,3-Butadiene-1-carbamate (59, 1) Benzyl Chloromethyl Ether (52, 16) 1-Benzylindole (54, 58) N-Alkylindoles from the Alkylation of Sodium Indolide in Hexamethylphosphoric Triamide: 1-Benzylindole (54, 60) 3-Alkylated and 3-Acylated Indoles from a Common Precursor: 3-Benzylindole and 3-Benzoylindole (56, 8) Alkylation of Isoquinolines via 2-Benzoyl-1,2-dihydroisoquinaldonitriles: 1-Benzylisoquinoline (56, 19) The Formation and Alkylation of Specific Enolate Anions from an Unsymmetrical Ketone: 2-Benzyl-2-methylcyclohexanone and 2-Benzyl-6-methylcyclohexanone (52, 39) Sulfide Synthesis: Benzyl Sulfide (58, 138) Bicyclo[1.1.0]butane (51, 55) Boranes in Functionalization of Dienes to Cyclic Ketones: Bicyclo[3.3.1]nonan-9-one (58, 24) Bicyclo[3.2.1]octan-3-one (51, 60) Bicyclo[2.1.0]pent-2-ene (55, 15) Dehydroxylation of Phenols; Hydrogenolysis of Phenolic Ethers: Biphenyl (51, 82) Controlled-Potential Electrolytic Reduction: 1,1-Bis(bromomethyl)cyclopropane (52, 22) Bis(trifluoromethyl)diazomethane (50, 6) Bis[2,2,2-trifluoro-1-phenyl-1-(trifluoromethyl)ethoxy] Diphenyl Sulfurane (57, 22) Acyloin Condensation in which Chlorotrimethylsilane is Used as a Trapping Agent: 1,2-Bis(trimethylsilyloxy)cyclobutene and 2-Hydroxycyclobutanone (57, 1) 2-Bornene (51, 66) Selective alpha-Bromination of an Aralkyl Ketone with Phenyltrimethylammonium Tribromide: 2-Bromoacetyl-6-methoxynaphthalene and 2,2-Dibromoacetyl-6-methoxynaphthalene (53, 111) Mercury(II) Oxide-Modified Hunsdiecker Reaction: 1-Bromo-3-chlorocyclobutane (51, 106) para-Bromination of Aromatic Amines: 4-Bromo-N,N-dimethyl-3-(trifluoromethyl)aniline (55, 20) Bromohydrins from Alkenes and N-Bromosuccinimide in Dimethyl Sulfoxide; erythro-2-Bromo-1,2-diphenylethanol (59, 16) Chain Elongation of Alkenes via gem-Dihalocyclopropanes: 2-Bromo-3,3-diphenyl-2-propen-1-yl acetate (56, 32) 2-Bromohexanoyl Chloride (55, 27) 1-Bromo-3-methyl-2-butanone (55, 24) trans, trans-1,3-Butadiene-1,4-diyl Diacetate (50, 24) A New Reagent for tert-Butoxycarbonylation: 2-tert-Butoxycarbonyloxyimino-2-phenylacetonitrile (59, 95) tert-Butoxycarbonyl-l-proline (53, 25) tert-Butyl Azidoformate (50, 9; 57, 122) tert-Butylcyanoketene (55, 32) cis-4-tert-Butylcyclohexanol (50, 13) Polymeric Carbodiimide. Moffat Oxidation: 4-tert-Butylcyclohexanone (56, 99) Oxidation of Alcohols by Methyl Sulfide- N-Chlorosuccinimide- Triethylamine: 4-tert-Butylcyclohexanone (58, 122) 2-tert-Butyl-1,3-diaminopropane (53, 21) Photochemical Ring-Contraction of 2-Ethoxypyrrolin-5-ones to Cyclopropanone Derivatives: tert-Butyl N-(1-Ethoxycyclopropyl)carbamate (59, 132) Phase-Transfer Hofmann Carbylamine Reaction: tert-Butyl Isocyanide (55, 96) Sulfide Synthesis in Preparation of Unsymmetrical Dlalkyl Disulfides: sec-Butyl Isopropyl Disulfide (58, 147) 3-Butyl-2-Methylhept-1-en-3-ol (52, 19) Monoalkylation of alpha,beta-Unsaturated Ketones via Metalloenamines: 1-Butyl-10-methyl-DELTA1(9)-2-octalone (57, 69) beta-Diketones from Methyl Alkyl Ketones: 3-n-Butyl-2,4-pentanedione (51, 90) Secondary and Tertiary Alkyl Ketones from Carboxylic Acid Chlorides and Lithium Phenylthio(alkyl)cuprate Reagents: tert-Butyl Phenyl Ketone (55, 122) Removal of Nalpha-Benzyloxycarbonyl Groups from Sulfur-Containing Peptides by Catalytic Hydrogenation in Liquid ammonia: O-tert-Butyl-L-seryl-S-tert-butyl-l-cysteine tert-Butyl Ester (59, 159) Esterification of Hindered Alcohols: tert-Butyl p-Toluate (51, 96) Peptide Syntheses Using N-Ethyl-5-phenylisoxazolium-3'-sulfonate: Carbobenzoxy-L-asparaginyl-L-leucine Methyl Ester and N-Carbobenzoxy-3-hydroxy-L-prolylglycylglycine Ethyl Ester (56, 88) Carbonyl Cyanide (51, 70) 3-Chlorocyclobutanecarboxylic Acid (51, 73) (z)-4-Chloro-4-hexenyl Trifluoroacetate (57, 26) m-Chloroperbenzoic Acid (50, 15) 3-(4-Chlorophenyl)-5-(4-Methoxyphenyl)Isoxazole (55, 39) alpha-Chloro Enamines, Reactive Intermediates for Synthesis: 1-Chloro-N,N,2-trimethylpropenylamine (59, 26) Modified Clemmensen Reduction: Cholestane (53, 86) Conjugate Reduction of alpha,beta-Unsaturated p-Toluenesulfonylhydrazones to Alkenes with Catecholborane: 5beta-Cholest-3-ene (59, 42) 5beta-Cholest-3-Ene-5-Acetaldehyde (54, 71) 18-Crown-6 (57, 30) Cinnamonitrile (50, 18) Preparation of Cyano Compounds Using Alkylaluminum Intermediates: 1-Cyano-6-methoxy-3,4-Dihydronaphthalene (52, 96) Cyclobutadieneiron Tricarbonyl (50, 21) Aldehydes from acid Chlorides by Reduction of Ester-mesylates with Sodium Borohydride: Cyclobutanecarboxaldehyde (51, 11) Cyclic Ketones from 1,3-Dithiane: Cyclobutanone (51, 76) Cyclobutanone from Methylenecyclopropane via Oxaspiropentane (57, 36) Cyclobutanone Via Solvolytic Cyclization (54, 84) One-carbon Ring Expansion of Cycloalkanones to Conjugated Cycloalkenones: 2-Cyclohepten-1-one (59, 113) Nitriles from Ketones: Cyclohexanecarbonitrile (58, 101) Aldehydes from Olefins: Cyclohexanecarboxaldehyde (57, 11) Catalytic Osmium Tetroxide Oxidation of Olefins: cis-1,2-Cyclohexanediol (58, 43) Stereoselective Hydroxylation with Thallium(i) Acetate and Iodine: trans- and cis-1,2-Cyclohexanediols (59, 169) Cleavage of Methyl Ethers with Iodotrimethylsilane: Cyclohexanol from Cyclohexyl Methyl Ether (59, 35) Preparation of alpha,beta-Unsaturated Aldehydes via the Wittig Reaction: Cyclohexylideneacetaldehyde (53, 104) Cyclopropenone (57, 41) Cyclopropyldiphenylsulfonium Tetrafluoroborate (54, 27) Ring Contraction via a Favorskii-Type Rearrangement: Cycloundecanone (56, 107) Hydrogenation of Aromatic Nuclei: 1-Decalol (51, 103) Oxidation with the Chromium Trioxide-Pyridine Complex Prepared in situ: 1-Decanal (55, 84) Reduction of Alkyl Halides and Tosylates with Sodium Cyanoborohydride in Hexamethylphosphoric Triamide (HMPA): A. 1-Iododecane to n-Decane B. 1-Dodecyl Tosylate to n-Dodecane (53, 107) Diamantane: Pentacyclo[7.3.1.14,12.02,7.06,11]tetradecane (53, 30) Macrocyclic Diimines: 1,10-dlazacycloCtadecane (54, 88) Dlazoacetophenone (53, 35) 2-diazocycloalkanones: 2-diazocyclohexanone (51, 86) 2-diazopropane (50, 27) Macrocyclic Polyethers: Dibenzo-18-crown-6 Polyether and Dicyclohexyl-18-crown-6 Polyether (52, 66) 1,2-Diaroylcyclopropanes: trans-1,2-Dibenzoylcyclopropane (52, 33) alpha, -Dibromodibenzyl Sulfone (50, 31) Phosphine-Nickel Complex Catalyzed Cross-Coupling of Grignard Reagents with Aryl and Alkenyl Halides: 1,2-Dibutylbenzene (58, 127) Oxidation with Bis(Salicylidene)ethylenediiminocobalt(II) (Salcomine); 2,6-Di-tert-butyl-p-benzoquinone (57, 78) Diazo Transfer by Means of Phase-transfer Catalysis: Di-tert-Butyl Diazomalonate (59, 66) Di-tert-butyl Dicarbonate (57, 45) cis-3,4-Dichlorocyclobutene (50, 36) cis-Dichloroalkanes from Epoxides: cis-1,2-Dichlorocyclohexane (58, 64) 2,3-Dicyanobutadiene as a Reactive Intermediate by in situ Generation from 1,2-Dicyanocyclobutene: 2,3-Dicyano-1,4,4a,9a-tetrahydrofluorene (58, 67) Dideuteriodiazomethane (53, 38) Diethylaluminum cyanide (52, 90) Diethylaminosulfur trifluoride (57, 50) Diethyl tert-Butylmalonate (50, 38) 2-Trimethylsilyloxy-1,3-butadiene as a Reactive Diene: Diethyl trans-4-Trimethylsilyloxy-4-cyclohexene-1,2-dicarboxylate (58, 163) Diethyl 2-(Cyclohexylamino)vinylphosphonate (53, 44) Radical Anion Arylation: Diethyl Phenylphosphonate (58, 134) Diethyl trans-delta4-Tetrahydrophthalate (50, 43) Homogeneous Catalytic Hydrogenation: Dihydrocarvone (53, 63) trans-1,2-Dihydrophthalic Acid (50, 50) 5,6-Dihydro-2H-pyran-2-one and 2H-Pyran-2-One (56, 49) 2,4-Dimethoxybenzonitrile (50, 52) Biaryls from Simple Arenes via Organotellurium Intermediates; 4,4'-Dimethoxy-1,1'-Biphenyl (57, 18) 6,7-Dimethoxy-3-Isochromanone (55, 45) Regioselective Mannich Condensation with Dimethyl(methylene)ammonium Trifluoroacetate: 1-Dimethylamino-4-methyl-3-pentanone (59, 153) Directed Lithiation of Aromatic Compounds: (2-Dimethylamino-5-methylphenyl)diphenylcarbinol (53, 56) Use of Dipotassium Nitrosodisulfonate (fremy's Salt): 4,5-Dimethyl-o-Benzoquinone (52, 88) 1,2-Dimethylcyclobutenes by Reductive Ring-Contraction of Sulfolanes: cis-7,8-Dimethylbicyclo[4.2.0]oct-7-Ene (57, 53) 4,4'-Dimethyl-1,1'-biphenyl (55, 48) N,N-Dimethyl-5beta-cholest-3-Ene-5-acetamide (54, 77) Conversion of Esters to Amides with Dimethylaluminum Amides: N,N-Dimethylcyclohexanecarboxamide (59, 49) 4,4-Dimethyl-2-Cyclohexen-1-one (53, 48) Reductive Amination with Sodium Cyanoborohydride: N,N- Dimethylcyclohexylamine (52, 124) N,N-Dimethyldodecylamine Oxide (50, 56) Dimethyl Nitrosuccinate (57, 60) Dimethyl 2,3-Pentadienedioate (57, 62) Allylically Transposed Amines from Allylic Alcohols; 3,7-Dimethyl-1,6-octadien-3-amine (58, 4) Bicyclic Ketones for The Synthesis of Tropinoids: 2alpha,4alpha-Dimethyl-8-oxabicyclo[3.2.1]oct-6-en-3-one (58, 17) 2,2-Dimethyl-4-Phenylbutyric Acid (50, 58) Cyclopentenones from alpha,alpha'-Dibromoketones and Enamines: 2,5-Dimethyl-3-phenyl-2-cyclopenten-1-one (58, 56) Alkylations of Aldehydes via Reaction of the Magnesioenamine Salt of an Aldehyde: 2,2-Dimethyl-3-phenylpropionaldehyde (54, 46) 3,5-Dinitrobenzaldehyde (53, 52) 2,3-Diphenyl-1,3-butadiene (50, 62) Reagents for Synthesis of Organoselenium Compounds: Diphenyl Diselenide and Benzeneselenenyl Chloride (59, 141) Aromatic Hydrocarbons from Aromatic Ketones and Aldehydes: 1,1-Diphenylethane (55, 7) Nucleophilic alpha-sec-Aminoalkylation: 2-(Diphenylhydroxymethyl)pyrrolidine (58, 113) Diphenylketene (52, 36) Alkenes via Hofmann Elimination: Use of Ion-Exchange Resin for Preparation of Quaternary Ammonium Hydroxides: Diphenylmethyl Vinyl Ether (55, 3) 2,3-Diphenylvinylene Sulfone (50, 65) 1,3-Dithiane (50, 72) 2,2'-Dithienyl Sulfide (50, 75) Selective Epoxidation of Terminal Double Bonds: 10, 11-Epoxyfarnesyl Acetate (56, 112) 1-Ethoxy-1-butyne (57, 65) Demethylation of Methyl Aryl Ethers: 4-Ethoxy-3-hydroxybenzaldehyde (56, 44) Carbine Generation by alpha-Elimination with Lithium 2,2,6,6-Tetramethylpiperidide: 1-Ethoxy-2-p-tolylcyclopropane (58, 37) Esterification of Carboxylic Acids with Trialkyloxonium Salts; Ethyl and Methyl 4-Acetoxybenzoates (56, 59) ortho-Alkylation of Anilines: Ethyl 4-Amino-3-Methylbenzoate (56, 15) Ethyl 5beta-Cholest-3-ene-5-acetate (54, 74) Free-Radical Cyclization: Ethyl 1-Cyano-2-Methylcyclohexanecarboxylate (55, 57) 2,2-(Ethylenedithio)cyclohexanone (54, 37) A General Synthesis of 4-Isoxazolecarboxylic Esters: Ethyl 3-Ethyl-5-methyl-4-isoxazolecarboxylate (53, 59) 3-Alkyl-1-alkynes Synthesis: 3-Ethyl-1-hexyne (58, 1) beta-Hydroxy Esters from Ethyl Acetate and Aldehydes or Ketones: Ethyl 1-Hydroxycyclohexylacetate (53, 66) Indoles from Anilines: Ethyl 2-Methylindole-5-carboxylate (56, 72) Stereoselective Synthesis of Trisubstituted Olefins: Ethyl 4-Methyl-(E)-4,8-nonadienoate (53, 116) Metalation of 2-Methylpyridine Derivatives: Ethyl 6-Methylpyridine-2-acetate (52, 75) Ethyl 1-Naphthylacetate (50, 77) Ethyl (E)-3-Nitroacrylate [Replaced by Methyl (E)-3-Nitroacrylate] (56, 65; replaced) gamma-Ketoesters from Aldehydes via Diethyl Acylsuccinates: Ethyl 4-oxohexanoate (58, 79) Ethyl Pyrrole-2-Carboxylate (51, 100) Thiazoles from Ethyl Isocyanoacetate and Thiono Esters: Ethyl Thiazole-4-carboxylate (59, 183) Carboxylation of Aromatic Compounds: Ferrocenecarboxylic Acid (56, 28) Fluorinations with Pyridinium Polyhydrogen Fluoride Reagent: 1-Fluoroadamantane (58, 75) Aldehydes from Aromatic Nitriles: 4-Formylbenzenesulfonamide (51, 20) Geranyl Chloride (54, 63) Allylic Chlorides from Allylic Alcohols: Geranyl Chloride (54, 68) Glutaconaldehyde Sodium Salt From Hydrolysis of Pyridinium-1-sulfonate (59, 79) Aldehydes from Primary Alcohols by Oxidation with Chromium Trioxide: Heptanal (52, 5) Conversion of Nitro to Carbonyl by Ozonolysis of Nitronates: 2,5-Heptanedione (56, 36) Macrocyclic Polyamines: 1,4,7,10,13,16-Hexaazacyclooctadecane (58, 86) Cuprous Ion-Catalyzed Oxidative Cleavage of Aromatic o-Diamines by Oxygen:(Z,Z)-2,4-Hexadienedinitrile (57, 33) Hexafluoroacetone Imine (50, 81) 3-Trimethylsilyl-3-buten-2-one as Michael Acceptor for Conjugate Addition-Annelation: cis-4,4a,5,6,7,8-Hexahydro-4a,5-dimethyl-2(3H)-naphthalenone (58, 158) Nitrones for Intramolecular 1,3-Dipolar Cycloadditions: Hexahydro-1,3,3,6-tetramethyl-2,1-benzisoxazoline (58, 106) (E)-4-Hexen-1-ol (55, 62) Fragmentation of alpha,beta-Epoxyketones to Acetylenic Aldehydes and Ketones: Preparation of 2,3-Epoxycyclohexanone and its Fragmentation to 5-Hexynal (55, 52) gamma-Hydroxy-alpha,beta-Unsaturated Aldehydes via 1,3-Bis(methylthio)allyllithium: trans-4-Hydroxy-2-hexenal (54, 19) 17beta-Hydroxy-5-oxo-3,5-seco-4-norandrostane-3-carboxylic Acid (55, 67) Directed Aldol Condensations: threo-4-Hydroxy-3-phenyl-2-heptanone (54, 49) Macrolides from Cyclization of omega-Bromocarboxylic Acids: 11-Hydroxyundecanoic Lactone (58, 98) Direct Iodination of Polyalkylbenzenes: Iododurene (51, 94) trans-Iodopropenylation of Alkyl Halides: (E)-1-Iodo-4-phenyl-2-butene (56, 77) 2-Iodo-p-xylene (55, 70) cis-alpha,beta-Unsaturated Acids: Isocrotonic Acid (53, 123) Trichloromethyl Chloroformate as a Phosgene Equivalent: 3-Isocyanatopropanoyl Chloride (59, 195) Hydroboration of Olefins: (+)-Isopinocampheol [Replaced by ( - )-Isopinocampheol] (52, 59) ( - )-Isopinocampheol (New) Reaction of Aryl Halides with PI-Allylnickel Halides: Methallylbenzene (52, 115) Sulfonyl Cyanides: Methanesulfonyl Cyanide (57, 88) 1,6-Methano[10]annulene (54, 11) Vinyl Sulfides from Thioacetals with Copper(I) Trifluoromethanesulfonate: (Z)-2-Methoxy-1-phenylthio-1,3-butadiene (59, 202) 6-Methoxy-beta-tetralone (51, 109) Methyl Groups by Reduction of Aromatic Carboxylic Acids with Trichlorosilane-tri-n-propylamine: 2-Methylbiphenyl (56, 83) 1-d-Aldehydes from Organometallic Reagents: 2-Methylbutanal-1-d (51, 31) Preparation of Vinyl Trifluoromethanesulfonates: 3-methyl-2-buten-2-yl Triflate (54, 79) Preparation and Reductive Cleavage of Enol Phosphates: 5-Methylcoprost-3-Ene (52, 109) Oxymercuration-Reduction: Alcohols from Olefins: 1-Methylcyclohexanol (53, 94) Reductive Cleavage of Allylic Alcohols, Ethers, or Acetates to Olefins: 3-Methylcyclohexene (56, 101) gamma-Ketoesters to Prepare Cyclic Diketones: 2-Methyl-1,3-cyclopentanedione (58, 83) Sulfide Contraction via Alkylative Coupling: 3-Methyl-2,4-Heptanedione (55, 127) Isoxazole Annelation Reaction: 1-Methyl-4,4a,5,6,7,8-Hexahydronaphthalen-2(3H)-one (53, 70) Addition of Organolithium Reagents to Allyl Alcohol: 2-Methyl-1-Hexanol (55, 1) Conversion of Primary Alcohols to Urethanes via the Inner Salt of Methyl (carboxysulfamoyl)Triethylammonium Hydroxide: Methyl n-Hexylcarbamate (56, 40) Methyl 2-Alkynoates from 3-Alkyl-2-pyrazolin-5-ones: Methyl 2-Hexynoate (55, 73) Methyl (trans-2-Iodo-1-Tetralin)carbamate (51, 112) Methyl Nitroacetate (55, 77) Methyl (E)-3-Nitroacrylate (New) 2-Methyl-2-nitrosopropane and Its Dimer (52, 77) Nucleophilic Acylation with Disodium Tetracarbonylferrate: Methyl 7-Oxoheptanoate and Methyl 7-Oxooctanoate (59, 102) Aldehydes from Allylic Alcohols and Phenylpalladium Acetate: 2-Methyl-3-phenylpropionalde (51, 17) Endocyclic Enamine Synthesis: N-Methyl-2-phenyl-DELTA2-tetrahydropyridine (54, 93) Hydrogenolysis of Carbon-Halogen Bonds with Chromium(II)-en Perchlorate: Naphthalene from 1-Bromonaphthalene (52, 62) Thiophenols from Phenols: 2-Naphthalenethiol (51, 139) S(-)-alpha-(1-Naphthyl)ethylamine (55, 80) Alkyl Iodides: Neopentyl Iodide and Iodocyclohexane (51, 44) Sulfide Synthesis in Preparation of Dialkyl and Alkyl Aryl Sulfides: Neopentyl Phenyl Sulfide (58, 143) 4-Nitrobenzyl Fluoride (57, 72) 1-Nitrocyclooctene (50, 84) Formation and Photochemical Wolff Rearrangement of Cyclic alpha-Diazo Ketones: D-Norandrost-5-en-3beta-ol-16-carboxylic Acids (52, 53) Highly Reactive Magnesium for the Preparation of Griignard Reagents: 1-Norbornanecarboxylic Acid (59, 85) DELTA9,10-Octalin (50, 88) 2,2,7,7,12,12,17,17-Octamethyl-21,22,23,24-tetraoxaperhydroquaterene (57, 74) Orcinol Monomethyl Ether (53, 90) 1,6-Oxido[10]annulene (55, 86) Cyanide-Catalyzed Conjugate Addition of Aryl Aldehydes: 4-Oxo-4-(3-pyridyl)butyronitrile (59, 53) Aldehydes from sym-Trithlane: n-Pentadecanal (51, 39) (Pentafluorophenyl)acetonitrile (57, 80) Pentafluorophenylcopper Tetramer, a Reagent for Synthesis of Fluorinated Aromatic Compounds (59, 122) trans-3-Penten-2-one (51, 115) Arene Oxide Synthesis: Phenanthrene-9,10-oxide (58, 12) Free-Radical Alkylation of Quinones: 2-Phenoxymethyl-1,4-Benzoquinone (56, 68) 3-Phenyl-2H-azirine-2-carboxaldehyde (57, 83) Phase-Transfer Alkylation of Nitriles: 2-Phenylbutyronitrile (55, 91) Directed Aldol Condensations: beta- Phenylcinnamaldehyde (50, 66) Aldehydes from 2-Benzyl-4,4,6-Trimethyl-5,6-dihydro-1,3(4H)-oxazine: 1-Phenylcyclopentanecarboxaldehyde (51, 24) Amines from Mixed Carboxylic-Carbonic Anhydrides: 1-Phenylcyclopentylamine (51, 48) cis-2-Phenylcyclofropanecarboxylic Acid (50, 94) Substitution of Aryl Halides with Copper(i) Acetylides: 2-Phenylfuro[3,2-b]pyridine (52, 128) Ketones and Alcohols from Organoboranes: Phenyl Heptyl Ketone, 1-Hexanol, and 1-Octanol (53, 77) 1-Phenyl-1,4-pentadiyne and 1-Phenyl-1,3-pentadiyne (50, 97) Phenylation with Diphenyliodonium Chloride; 1-Phenyl-2,4-pentanedione (51, 128) 1-Phenyl-4-phosphorinanone (53, 98) 4-Phenyl-1,2,4-triazoline-3,5-dione (51, 121) 2-Phenyl-2-vinylbutyronitrile (55, 99) Boranes in Functionalization of Olefins to Amines: 3-Pinanamine (58, 32) Allylic Oxidation with Hydrogen Peroxide-Selenium Dioxide: trans-Pinocarveol (56, 25) Base-Induced Rearrangement of Epoxides to Allylic Alcohols: trans-Pinocarveol (53, 17) Polymeric Carbodiimide. Preparation (56, 95) Alkynes via Phase Transfer - Catalyzed Dehydrohalogenation: Propiolaldehyde Diethyl Acetal (59, 10) Rearrangement of Bridgehead Alcohols to Polycyclic Ketones by Fragmentation-Cyclization: 4-Protoadamantanone (Tricyclo[4.3.1.03.8]Decan-4-One) (59, 147) Quadricyclane (51, 133) 1,2,3,4-Tetrahydro-beta-Carboline (51, 136) Aziridines from beta-Iodocarbamates: 1,2,3,4-Tetrahydronaphthalene(1,2)Imine (51, 53) 2,3,4,5-Tetrahydropyridine Trimer (56, 118) 3,3,6,6-Tetramethoxy-1,4-Cyclohexadiene (57, 92) 2,2,3,3-Tetramethyliodocyclopropane (52, 132) 4H-1,4-Thiazine l,1-Dioxide (52, 135) 2-Thiophenethiol (50, 104) p-Tolylsulfonyldiazomethane (57, 95) p-Tolylsulfonylmethyl Isocyanide (57, 102) Tri-tert-Butylcyclopropenyl Tetrafluoroborate (54, 97) Tricarbonyl[2,3,4,5-eta)-2,4,-Cyclohexadien-1-One]Iron and Tricarbonyl[(1,2,3,4,5-eta)-2-Methyoxy-2,4-Cyclohexadien-1-Yl]Iron(1+) Hexafluorophosphate(1 - ) from Anisole (57, 107) Alkylation of Dimedone with a Tricarbonyl(diene)Iron Complex: Tricarbonyl[2-[2,3,4,5-eta)-4-Methoxy-2,4-Cyclohexadien-1-yl]-5,5-Dimethyl-1,3-Cyclohexanedione]iron (57, 16) Cyclobutadiene in Synthesis: endo-Tricyclo[4.4.0.02,5]Deca-3,8-Diene-7,10-Dione (55, 43) Trifluoroacetylation of Amines and Amino Acids Under Neutral, Mild Conditions: N-Trifluoroacetanilide and N-Trifluoroacetyl-L-Tyrosine (56, 122) Aldehydes from Acid Chlorides by Modified Rosenmund Reduction: 3,4,5-Trimethoxybenzaldehyde (51, 8) Oxidation with the Nitrosodisulfonate Radical. I. Preparation and Use of Disodium Nitrosodisulfonate: Trimethyl-p-Benzoquinone (52, 83) 2,2-(Trimethylenedithio)Cyclohexanone (54, 39) Trimethylene Dithiotosylate and Ethylene Dithiotosylate (54, 33) Trimethyloxonium Tetrafluoroborate (51, 142) 3,5,5-Trimethyl-2-(2-Oxopropyl)-2-Cyclohexen-1-One (57, 113) Aldehydes by Oxidation of Terminal Olefins with Chromyl Chloride: 2,4,4-Trimethylpentanal (51, 4) Trimethylsilyl Azide (50, 107) 3-Trimethylsilyl-3-Buten-2-One: a Michael Acceptor (58, 152) Tropolone (57, 117) Preparation of Alkenes by Reaction of Lithium Dipropenylcuprates with Alkyl Halides: (E)-2-Undecene (55, 103; deleted) General Index Frmula Index Hazard Index Author Index Concordance Index
Responsibility: editorial board, Wayland E. Noland, editor-in chief ...

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