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Organic Trace Analysis by Liquid Chromatography.

Author: James Lawrence
Publisher: Oxford : Elsevier Science, 1981.
Edition/Format:   eBook : Document : EnglishView all editions and formats
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Organic Trace Analysis by Liquid Chromatography.
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Genre/Form: Electronic books
Additional Physical Format: Print version:
Lawrence, James.
Organic Trace Analysis by Liquid Chromatography.
Oxford : Elsevier Science, ©1981
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: James Lawrence
ISBN: 9780323157025 0323157025
OCLC Number: 831116555
Description: 1 online resource (301 pages)
Contents: Front Cover; Organic Trace Analysis by Liquid Chromatography; Copyright Page; Dadication; Table of Contents; Preface; Chapter 1. General Considerations in Developing a Trace Analytical Technique Employing Liquid Chromatography; I. Liquid Chromatography versus Gas Chromatography; II. Residue Analysis versus Formulations Analysis; III. Pump and Injector Requirements; IV. Detectors; V. Chromatography; VI. Extraction and Cleanup; VII. Minimum Detectable Levels; VIII. Matrix Effects; IX. Use of Derivatization; X. Microprocessors and Automation; References; Chapter 2. Pumping Systems. I. IntroductionII. Constant Volume Pumps; III. Constant Pressure Pumps; IV. Gradient Elution; V. Comparison of Pumping Systems; Chapter 3. Sampling Technique and Injection Ports; I. Effect of Sample Solution on Peak Shape; II. Requirements for Trace Analysis; III. Types of Injection Ports; References; Chapter 4. Chromatography Columns and Packing Materials; I. Requirements for Trace Analysis; II. Pellicular versus Microparticulate Porous Packings; III. Commercial Prepacked Columns; IV. Column Packing Techniques; V. Stationary-Phase Materials; References; Chapter 5. Detectors; I. Introduction. II. General Detector RequirementsIII. Photometric Detectors; IV. Electrochemical Detectors; V. Solute Transport Detectors; VI. Refractive Index Detectors; VII. Mass Spectrometer; VIII. Other Detectors; References; Chapter 6. Chromatography Theory; I. Fundamental Principles; II. Adsorption Chromatography; III. Partition Chromatography; IV. Macroreticular Resins; V. Ion-Pair Chromatography; VI. Ion-Exchange Chromatography; VII. Ion Chromatography; VIII. Gel Permeation Chromatography; IX. Ligand-Exchange Chromatography; X. Charge-Transfer Chromatography; References. Chapter 7. Chemical DerivatizationI. Introduction; II. UV-Absorbance Derivatization; III. Fluorescence Derivatization; IV. Derivatization for Other Detection Modes; V. Postcolumn Reactions; References; Chapter 8. Sample Extraction and Cleanup; I. Considerations; II. Sample Extraction; III. Sample Cleanup; IV. Column Chromatography; V. Thin-Layer Chromatography; VI. Distillation; VII. Low-Temperature Precipitation; References; Chapter 9. Approach to Method Development and RoutineAnalysis; I. Choosing the Best Chromatography System; II. Analysis Time and Interfering Peaks. III. Qualitative and Quantitative Analysis and ConfirmationIV. Automation; V. Integration of LC with Other Analytical Techniques; VI. LC as a Cleanup Technique; References; Chapter 10. Applications; I. Introduction; II. Clinical (Biological Fluids and Tissues; III. Environmental; IV. Foods; References; Index.

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Organic Trace Analysis by Liquid Chromatography.

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