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Perchlorate ester: Preparation and polymerization

Author: J Radell; J W Connolly; Aeronautical Systems Division (U.S.).
Publisher: Wright-Patterson AFB, Ohio : Aeronautical Systems Division, Air Force Systems Command, United States Air Force, 1961.
Series: Aeronautical Systems Division (U.S.).; Technical Report
Edition/Format:   Book : National government publication : EnglishView all editions and formats
Database:WorldCat
Summary:
Epiperchloratohydrin (I) was synthesized and polymerized; although covalent perchlorates are known to be hydrolytically unstable. Compound (I), dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound (I) before and after polymerization was explosive and required special care.
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Additional Physical Format: Online version:
Radell, J.
Perchlorate ester.
Wright-Patterson AFB, Ohio : Aeronautical Systems Division, Air Force Systems Command, United States Air Force, 1961
(OCoLC)728065692
Material Type: Government publication, National government publication
Document Type: Book
All Authors / Contributors: J Radell; J W Connolly; Aeronautical Systems Division (U.S.).
OCLC Number: 435787536
Notes: "September 1961."
AD0691014 (from http://www.dtic.mil).
PB-181363.
Research supported by the United States Air Force, Air Force Systems Command, Directorate of Materials and Processes.
Description: iii, 4 p. : 28 cm.
Series Title: Aeronautical Systems Division (U.S.).; Technical Report
Responsibility: J. Radell, J. W. Connolly.

Abstract:

Epiperchloratohydrin (I) was synthesized and polymerized; although covalent perchlorates are known to be hydrolytically unstable. Compound (I), dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound (I) before and after polymerization was explosive and required special care.

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