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Perchlorate ester : preparation and polymerization

Author: Jack Radell; J W Connolly; United States. Air Force. Systems Command. Aeronautical Systems Division.; Wright-Patterson Air Force Base (Ohio)
Publisher: Wright-Patterson AFB, Ohio : Aeronautical Systems Division, Air Force Systems Command, United States Air Force, 1961.
Series: ASD technical report, 61-158.
Edition/Format:   Print book : National government publication : EnglishView all editions and formats
Database:WorldCat
Summary:
Epiperchloratohydrin (I) was synthesized and polymerized; although covalent perchlorates are known to be hydrolytically unstable. Compound (I), dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound (I) before and after polymerization was explosive and required special care.
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Additional Physical Format: Online version:
Radell, J.
Perchlorate ester.
Wright-Patterson AFB, Ohio : Aeronautical Systems Division, Air Force Systems Command, United States Air Force, 1961
(OCoLC)728065692
Material Type: Government publication, National government publication
Document Type: Book
All Authors / Contributors: Jack Radell; J W Connolly; United States. Air Force. Systems Command. Aeronautical Systems Division.; Wright-Patterson Air Force Base (Ohio)
OCLC Number: 435787536
Notes: "September 1961."
"Project No. 7360."
AD0691014 (from http://www.dtic.mil).
PB-181363.
Research supported by the United States Air Force, Air Force Systems Command, Directorate of Materials and Processes.
"This report was prepared jointly by the Radiation Studies Section, Radiation Branch, Physics Laboratory and the Chemistry Research Laboratory, Aeronautical Research Laboratories. The work was initiated under Project 7360. "The Chemistry and Physics of Materials", Task 73607, "High Energy Materials Phenomena", and was administered under the direction of the Directorate of Materials and Processes, Aeronautical Systems Division with Dr. Jack Radell and Captain J.W. Connelly acting as project engineers." -- Foreword.
"This report covers work done during the period 1 January 1960 to 1 January 1961." -- Foreword.
Description: iii, 4 pages ; 28 cm.
Series Title: ASD technical report, 61-158.
Responsibility: J. Radell, J.W. Connolly.

Abstract:

Epiperchloratohydrin (I) was synthesized and polymerized; although covalent perchlorates are known to be hydrolytically unstable. Compound (I), dissolved in benzene could be rapidly washed with water without causing major hydrolysis. A simple method for dehydrating silver perchlorate by an azeotropic distillation was used. Compound (I) before and after polymerization was explosive and required special care.

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