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Plant analysis procedures

Author: Erwin E J M Temminghoff; Victor J G Houba
Publisher: Dordrecht ; Boston : Kluwer Academic Publishers, ©2004.
Edition/Format:   Print book : English : 2nd edView all editions and formats
Summary:

Intended for the practising chemist who has to do a job in analysing plant material. This manual describes procedures for inorganic components, which frequently occur in the plant. It discusses more  Read more...

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Material Type: Internet resource
Document Type: Book, Internet Resource
All Authors / Contributors: Erwin E J M Temminghoff; Victor J G Houba
ISBN: 1402027699 9781402027697 1402029764 9781402029769
OCLC Number: 59081352
Notes: Revised edition of: Plant analysis manual, 1995.
Description: x, 179 pages : illustrations ; 25 cm
Contents: Preface.- 1. Introduction.- 1.1 Organisation Of This Manual. 1.2 Technical Remarks. 1.3 Sampling And Pretreatment. 2. Digestions.- 2.1 Digestion In Tubes With H2SO4 - Salicylic Acid - H2O2 And Selenium. For the determination of total Ca, K, Mg, Mn, N, N, Na, P and Zn. 2.2 Digestion In Flasks With H2SO4 - Salicylic Acid - H2O2. For the determination of total Ca, K, Mg, Mn, N, Na, P, and Zn. 2.3 Microwave Digestion With HNO3 - H2O2 - HF. For the determination of total Al, As, Ca, Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, P, Pb, S, Sb, Sn, V and Zn. 2.4 Digestion With HNO3 - H2O2 - HF.- For the determination of total Al, As, Ca, Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, P, Pb, S, Sb, Sn, V and Zn. 2.5 Digestion With HNO3.- For the determination of total S. 2.6 Digestion With HNO3 - HCLO4 - H2SO4.- For the determination of total Cd, Cu, Fe, Mn and Zn. 2.7 Digestion By Dry-Ashing Followed By Treatment With HF.-For the determination of total Al, As, Ca, Cd, Co, Cr, Cu, Fe, K, Mg, Mn, Na, Ni, P, Pb, S, Sb, Sn, V and Zn. 2.8 Digestion By Dry-Ashing In The Presence Of CAO. For the determination of total B. 3. Extractions.- 3.1 Extraction With Water. For the determination of Cl-, NO2-, NO3- and SO42- 3.2 Extraction With HF - HCL. For the determination of total B and Si. 4. Determinations.- 4.1 Determination Of Aluminium.- 4.1.A Determination Of Aluminium By Spectrophotometry. 4.1.B Determination Of Aluminium By ICP-OES. 4.1.C Determination Of Aluminium By ICP-MS. 4.2 Determination Of Arsenic.- 4.2.A Determination Of Arsenic By ICP-MS. 4.3 Determination Of Boron.- 4.3.A Determination Of Boron By Spectrophotometry. 4.3.B Determination Of Boron By ICP-OES. 4.4 Determination Of Calcium.- 4.4.A Determination Of Calcium By Flame AES. 4.4.B Determination Of Calcium By Flame AAS. 4.4.C Determination Of Calcium By ICP-OES. 4.5 Determination Of Cadmium.- 4.5.A Determination Of Cadmium By Flame AAS. 4.5.B Determination Of Cadmium By ICP-OES. 4.5.C Determination Of Cadmium By ETA-AAS. 4.5.D Determination Of Cadmium By ICP-MS. 4.6 Determination Of Chloride.- 4.6.A Determination Of Chloride By Coulometric Titration. 4.7 Determination Of Cobalt.- 4.7.A Determination Of Cobalt By ICP-OES. 4.7.B Determination Of Cobalt By ICP-MS. 4.8 Determination Of Chromium.- 4.8.A Determination Of Chromium By ICP-OES. 4.8.B Determination Of Chromium By ICP-MS. 4.9 Determination Of Copper.- 4.9.A Determination Of Copper By Flame AAS. 4.9.B Determination Of Copper By ICP-OES. 4.9.C Determination Of Copper By ETA-AAS. 4.9.D Determination Of Copper By ICP-MS. 4.10 Determination Of Iron.- 4.10.A Determination Of Iron By Flame AAS. 4.10.B Determination Of Iron By ICP-OES. 4.11 Determination Of Potassium.- 4.11.A Determination Of Potassium By Flame AES. 4.11.B Determination Of Potassium By ICP-OES. 4.12 Determination Of Magnesium.- 4.12.A Determination Of Magnesium By Flame AAS. 4.12.B Determination Of Magnesium By ICP-OES. 4.13 Determination Of Manganese.- 4.13.A Determination Of Manganese By Flame AAS. 4.13.B Determination Of Manganese By ICP-OES. 4.13.C Determination Of Manganese By ICP-MS. 4.14 Determination Of Nitrogen Fractions.- 4.14.A Determination Of Total Nitrogen By Spectrophotometry. 4.14.B Determination Of Total Nitrogen By SFA. 4.14.C Determination Of Nitrate (+ Nitrite) By SFA. 4.14.D Determination Of Nitrate-Nitrogen By ISE. 4.14.E Determination Of Nitrite By SFA. 4.15 Determination Of Sodium.- 4.15.A Determination Of Sodium By Flame AES. 4.15.B Determination Of Sodium By ICP-OES. 4.16 Determination Of Nickel.- 4.16.A Determination Of Nickel By Flame AAS. 4.16.B Determination Of Nickel By Flame AAS. 4.16.C Determination Of Nickel By ICP-MS. 4.17 Determination Of Phosphorus.- 4.17.A Determination Of Total Phosphorus By Spectrophotometry. 4.17.B Determination Of Total Phosphorus By SFA. 4.17.C Determination Of Total Phosphorus By ICP-OES. 4.18 Determination Of Lead.- 4.18.A Determination Of Lead By Flame AAS. 4.18.B Determination Of Lead By ICP-OES. 4.18.C Determination Of Lead By ETA-AAS. 4.18.D Determination Of Lead By ICP-MS. 4.19 Determination Of Sulphur Fractions.- 4.19.A Determination Of Total Sulphur By ICP-OES. 4.19.B Determination Of Sulphate By ICP-OES. 4.20 Determination Of Antimony.- 4.20.A Determination Of Antimony By ICP-MS. 4.21 Determination Of Silicon.- 4.21.A Determination Of Silicon By ICP-OES. 4.22 Determination Of Tin.- 4.22.A Determination Of Tin By ICP-MS. 4.23 Determination Of Vanadium.- 4.23.A Determination Of Vanadium By ICP-MS. 4.24 Determination Of Zinc.- 4.24.A Determination Of Zinc By Flame AAS. 4.24.B Determination Of Zinc By ICP-OES. 4.24.C Determination Of Zinc By ICP-MS.
Responsibility: edited by Erwin E.J.M. Temminghoff and Victor J.G. Houba.

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