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A practical guide to graphite furnace atomic absorption spectrometry

Author: David J Butcher; Joseph Sneddon
Publisher: New York : Wiley, ©1998.
Series: Chemical analysis, v. 149.
Edition/Format:   Print book : EnglishView all editions and formats
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Additional Physical Format: Online version:
Butcher, David J.
Practical guide to graphite furnace atomic absorption spectrometry.
New York : Wiley, ©1998
(OCoLC)610147785
Material Type: Internet resource
Document Type: Book, Internet Resource
All Authors / Contributors: David J Butcher; Joseph Sneddon
ISBN: 0471125539 9780471125532
OCLC Number: 37513020
Notes: "A Wiley-Interscience publication."
Description: xviii, 250 pages : illustrations ; 24 cm.
Contents: Chapter 1. Introduction --
Chapter 2. Theory --
2.1 Spectroscopy --
2.2 Introduction to atomic spectroscopy --
2.3 Quantitative considerations of transitions --
2.3.1 Population of atoms in a state : the Boltzmann distribution --
2.3.2 Einstein coefficients --
2.4 Electronic states of atoms --
2.4.1 Quantum numbers for electrons --
2.4.2 Coupling schemes, term symbols, and selection rules --
2.4.3 Atomic spectra --
2.5 Measures of transition strengths : transition probabilities and oscillator strengths --
2.6 Spectral profiles of absorption lines --
2.7 GFAAS analytical signal : absorbance --
2.8 Intensity of absorbance in terms of fundamental parameters --
2.9 Nature of the transient GFAAS signal : mechanism of atom formation in a graphite furnace --
2.9.1 Surface processes --
2.9.2 Heterogeneous solid-gas interactions --
2.9.3 Gas-phase chemistry --
2.9.4 Processes by which analyte is lost from the tube --
2.9.5 Monte Carlo simulations of atomization processes --
References --
Chapter 3. Quantitative GFAAS : Calibration --
3.1 General analytical methodology --
3.2 Calibration graphs --
3.3 Method of standard additions --
3.4 Method of internal standardization --
3.5 Absolute analysis --
References --
Chapter 4. Instrumentation --
4.1 Light sources --
4.1.1 Hollow cathode lamps --
4.1.2 Electrodeless discharge lamps --
4.1.3 Xenon arc lamps --
4.1.4 Semiconductor diode lasers --
4.2 Graphite furnace --
4.2.1 Graphite tube material and design --
4.2.2 Furnace heating cycle --
4.2.3 Methods of atomization --
4.3 Wavelength selectors --
4.3.1 Monochromators --
4.3.2 Échelle monochromators --
4.4 Detectors --
4.5 Signal processing, readout, and instrumental control --
4.6 Background correction --
4.6.1 Nearby line (two-line) method --
4.6.2 Continuum source method --
4.6.3 Self-reversal (Smith-Hieftje) method --
4.6.4 Zeeman effect method --
4.6.4.1 Inverse longitudinal ac Zeeman. 4.6.4.2 Inverse transverse ac Zeeman --
4.6.4.3 Inverse transverse dc Zeeman --
4.6.5 Comparison of background correction systems --
4.7 Graphite furnace atomic emission spectrometry --
4.8 Spectrometer designs --
4.8.1 Single-element instruments --
4.8.2 Multielement instruments --
References --
Chapter 5. Interference-Free Analysis --
5.1 Spectral interferences --
5.1.1 Spectral overlaps --
5.1.2 Background attenuation --
5.2 Chemical interferences --
5.3 Physical interferences --
References --
Chapter 6. Sample Preparation and Introduction --
6.1 Liquids --
6.2 Gases --
6.3 Solids --
6.3.1 Wet decomposition --
6.3.2 Combustion --
6.3.3 Fusion --
6.3.4 Summary of digestion procedures --
6.3.5 Solids analysis with slurry sampling --
6.3.6 Direct solid sampling --
6.3.7 Laser ablation --
6.4 Preconcentration/separation methods --
6.4.1 Extraction --
6.4.2. Chromatography --
6.4.3 Flow injection analysis --
6.4.4 Other preconcentration/separation methods --
6.5 Metal speciation --
References --
Chapter 7. Practical Hints on the Determination of Elements by GFAAS --
7.1 Applicability --
7.2 Sampling, sample storage, and sample preparation --
7.3 Quality control procedures --
7.4 Development of GFAAS methods --
7.5 Troubleshooting --
References --
Chapter 8. Commercial GFAAS Instrumentation: Types, Costs, and Training --
8.1 Types and costs of GFAAS instrumentation --
8.2 Consumables --
8.3 Service and maintenance --
8.4 Training --
Chapter 9. Future of GFAAS --
Appendix A. Historical background --
A.1 Early work in atomic spectroscopy (before 1955) --
A.2 Flame atomic absorption spectrometry --
A.3 Graphite furnace atomic absorption spectrometry --
References --
Appendix B. GFAAS Literature --
B.1 Books --
B.2 Periodicals --
B.3 Reviews --
B.4 Internet resources --
B.5 Applications of GFAAS --
References --
Appendix C. Conditions for GFAAS.
Series Title: Chemical analysis, v. 149.
Responsibility: David J. Butcher, Joseph Sneddon.
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