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Quantitation and mass spectrometric data of drugs and isotopically labeled analogs

Author: Ray H Liu; Sheng-Meng Wang; Dennis V Canfield
Publisher: Boca Raton : CRC Press, ©2010.
Edition/Format:   eBook : Document : EnglishView all editions and formats
Summary:

A reference for labs involved in the analysis of abused and therapeutic drugs that features more than 1500 full-scan mass spectra data tables. It illustrates approaches, mechanisms, and challenges  Read more...

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Genre/Form: Electronic books
Additional Physical Format: Print version:
Liu, Ray H.
Quantitation and mass spectrometric data of drugs and isotopically labeled analogs.
Boca Raton : CRC Press, ©2010
(DLC) 2009026283
(OCoLC)423572434
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: Ray H Liu; Sheng-Meng Wang; Dennis V Canfield
ISBN: 9781420094985 142009498X
OCLC Number: 680036363
Description: 1 online resource (xii, 498 pages) : illustrations
Contents: Part One. Isotopically Labeled Analog as Internal Standard for Drug Quantitation - Methodology Quantitation of Drug in Biological Specimen - Isotopically Labeled Analog of the Analyte as Internal Standard Introduction Significance of Accurate Quantitation Preferred Calibration Method Internal Standard and Quantitation Ions Inadequate Isotopic Purity - An Extrinsic Factor Cross-Contribution Derived from Ion Fragmentation Mechanism - An Intrinsic Factor Fitting Calibration Data 2H- Versus 13C-Analogs as Internal Standards Concluding Remarks References Isotopically Labeled Analog of the Analyte as Internal Standard for Drug Quantitation - Chemical Derivatization and Data Collection and Evaluation Introduction Chemical Derivatization Production of Most Favorable Ion-Pairs for Drug Quantitation Exemplar Studies Isotopically Labeled Analogs and Chemical Derivatization Groups Ion Intensity Cross-Contribution Data Full-Scan Mass Spectra Selected Ion Monitoring and Calculation of Cross-Contribution Data: Direct Measurement, Normalized Direct Measurement, Internal Standard Method, Standard Addition Method Assessing the Accuracy of Empirically Determined Cross-Contribution Data: Experimentally Observed Concentration, Theoretically Calculated Concentration, Comparing Empirically Derived and Theoretically Calculated Concentrations - Graphic Presentation, Summary Compilation of Full-Scan Mass Spectra and Ion Intensity Cross-Contribution Tables: Derivatization Procedures, Instrumentation, and Analytical Parameters Collection of Mass Spectrometric Data Ion Intensity Cross-Contribution Data Concluding Remarks References Part Two. Mass Spectra of Commonly Abused Drugs and Their Isotopically Labelled Analogs in Various Derivatization Forms Table of Contents for Appendix One Stimulants Opioids Hallucinogens Depressants/Hypnotics Antianxiety Agents Antidepressants Others Part Three. Cross-Contributions of Ion Intensity Between Analytes and Their Isotopically Labeled Analogs in Various Derivatization Forms Table of Contents for Appendix Two Stimulants Opioids Hallucinogens Depressants/Hypnotics Antianxiety Agents Antidepressants Others Index
Responsibility: Ray H. Liu, Sheng-Meng Wang, Dennis V. Canfield ; with the assistance of Meng-Yan Wu [and others].

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The information presented in this book is definitely of value to any laboratory engaged in toxicology analysis and the quantification of drugs. -Maria Reid, Royal Canadian Mounted Police, Canadian Read more...

 
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