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| Genre/Form: | Laboratory manuals |
|---|---|
| Document Type: | Book |
| All Authors / Contributors: |
Lutz F Tietze; Theophil Eicher; Ulf Diederichsen; Andreas Speicher |
| ISBN: | 9783527312238 3527312234 |
| OCLC Number: | 262902114 |
| Description: | XVI, 582 p. : ill. ; 24 cm. |
| Contents: | 1 C-C Bond formation. Introduction. 1.1 Nucleophilic addition to aldehydes, ketones, carboxylic acid derivatives (esters, anhydrides), and alpha,beta-unsaturated carbonyl compounds; carbonyl olefination. 1.1.1 (E)-Acetoxy-2-methyl-2-butenal. 1.1.2 (S)-2,3-Dimethylhex-5-en-3-ol. 1.1.3 (S)-5-Oxo-3,5-diphenylpentanoic acid methyl ester. 1.1.4 (S)-3-Phenylheptanoic acid. 1.1.5 Ethyl 8-chloro-4-methyl naphthalene-2-carboxylate. 1.1.6 ( )-4-Hydroxy-ar-himachalane. 1.1.7 Methylenecyclododecane. 1.2 Alkylation of aldehydes/ketones, carboxylic acids, and beta-dicarbonyl compounds. 1.2.1 (+)-(S)-4-Methylheptan-3-one. 1.2.2 (S)-2-Isopropylhex-4-yn-1-ol. 1.2.3 3-Oxo-5-phenylpentanoic acid methylester. 1.3 Reactions of the aldol and Mannich type. 1.3.1 Olivetol. 1.3.2 (+)-(7aS)-7,7a-Dihydro-7a-methyl-1,5(6H)-indanedione. 1.3.3 Cyclohexyl 2-benzoylamino-2-(2'-oxocyclohexyl) acetate. 1.3.4 (S)-1-Hydroxy-1,3-diphenyl-3-propanone. 1.3.5 [(1S,2R,6R)-2-Hydroxy-4-oxo-2,6-diphenyl]cyclohexane carboxylic acid ethyl ester. 1.4 Electrophilic and nucleophilic acylation. 1.4.1 (-)-Ethyl (1R)-1-methyl-2-oxocyclopentane-1-carboxylate. 1.4.2 Ethyl (S)- and (R)-2-hydroxy-4-phenylbutanoate. 1.4.3 Naproxen. 1.4.4 3-Benzoylcyclohexanone. 1.5 Reactions of alkenes via carbenium ions. 1.5.1 Piperine. 1.5.2 Cicloxilic acid. 1.5.3 beta-Ionone. 1.6 Transition-metal-catalyzed reactions. 1.6.1 (E)-4-Chlorostilbene. 1.6.2 2-Cyanomethyl-3',4'-dimethoxybiphenyl. 1.6.3 (2-Phenylethynyl)aniline. 1.6.4 3,3-Dimethylcyclohexanone. 1.7 Pericyclic reactions. 1.7.1 Tranylcypromine. 1.7.2 11,11-Difluoro-1,6-methano[10]annulene. 1.7.3 Dimethyl heptalene-1,2-dicarboxylate. 1.7.4 Dimethyl 1,8-bishomocubane-4,6-dicarboxylate. 1.7.5 alpha-Terpineol. 1.7.6 Bicyclo[2.2.2]octene derivative. 1.8 Radical reactions. 1.8.1 Ethyl 4,6,6,6-tetrachloro-3,3-dimethylhexanoate. 1.8.2 3-Bromophenanthrene. 2 Oxidation and reduction. 2.1 Epoxidation of C=C bonds. 2.1.1 Sharpless.Katsuki epoxidation. 2.1.2 Jacobsen epoxidation. 2.2 Dihydroxylation of C=C bonds. 2.2.1 Sharpless dihydroxylation. 2.3 Oxidation of alcohols to carbonyl compounds. 2.3.1 Swern oxidation. 2.3.2 Dess.Martin oxidation. 2.3.3 Perruthenate oxidation. 2.3.4 TEMPO oxidation. 2.4 Enantioselective reduction of ketones. 2.4.1 BINAL-H -Reduction of butyrophenone. 2.4.2 CBS-Reduction of acetophenone. 3 Heterocyclic compounds. Introduction. 3.1 Three- and four-membered heterocycles. 3.1.1 (S)-Propranolol. 3.1.2 Oxetane derivative. 3.1.3 Azetidin-2-one derivative. 3.2 Five-membered heterocycles. 3.2.1 2,4-Diphenylfuran. 3.2.2 3,4-Dimethylpyrrole. 3.2.3 4,6-Dimethoxybenzo[b]thiophene. 3.2.4 2-Phenylindole. 3.2.5 Melatonin. 3.2.6 3-(4-Methylbenzoylamino)-1-phenyl-4,5-dihydropyrazole. 3.2.7 Camalexin. 3.2.8 Microwave-assisted pyrazole synthesis. 3.3 Six-membered heterocycles 293 3.3.1 Azine and diazine syntheses with acetoacetate. 3.3.2 (R)-Salsolidine. 3.3.3 Epirizole. 3.3.4 Ras farnesyltransferase inhibitor. 3.3.5 ( )-Dihydrexidine. 3.4 Condensed heterocycles. 3.4.1 6-Ethoxycarbonylnaphtho[2,3-a]indolizine-7,12-quinone. 3.4.2 EGF-R-Pyrrolo[2,3-d]pyrimidine. 3.4.3 7-Phenyl-1,6-naphthyridine. 3.4.4 Caffeine. 3.4.5 Nedocromil analogon. 3.4.6 High-pressure reaction. 3.5 Other heterocyclic systems; heterocyclic dyes. 3.5.1 ( )-Samin. 3.5.2 Dibenzopyridino[18]crown-6. 3.5.3 Indigo. 3.5.4 Pyrvinium iodide. 3.5.5 2,3,7,8,12,13,17,18-Octamethylporphyrin. 3.5.6 Synthesis of a rotaxane. 4 Selected natural products 4.1 Alkaloids. Introduction. 4.1.1 Hirsutine. 4.1.2 rac-2,3-Dimethoxyberbine. 4.1.3 Buflavine. 4.2 Isoprenoids. Introduction. 4.2.1 ( )-trans-Chrysanthemic acid. 4.2.2 Nerol. 4.2.3 (-)-Menthol. 4.2.4 Artemisia ketone. 4.2.5 Veticadinol. 4.2.6 all-trans-Vitamin A acetate. 4.3 Carbohydrates. Introduction. 4.3.1 Synthesis of glycosyl donors. 4.3.2 Glycosylations of glucosyl donors with cyclopentanol. 4.4 Amino acids and peptides. Introduction. 4.4.1 N-Boc-N-methyl-(S)-alanyl nucleo amino acid. 4.4.2 (S)-Homoproline. 4.4.3 Amino acid resolution with amino acylase. 4.4.4 gamma,delta-Unsaturated alpha-amino acids. 4.4.5 Passerini hydroxyamide. 4.4.6 Aspartame. 4.4.7 Ugi dipeptide ester. 4.4.8 Solid-phase synthesis of beta-peptides. 4.5 Nucleotides and oligonucleotides. Introduction. 4.5.1 2',3'-Dibenzoyl-6'-O-DMT-β-D-glucopyranosyl-uracil 4'-O-phosphoramidite. 4.5.2 Solid-phase Synthesis of Nucleic acids. 5 Index of reactions. 6 Index of products. 7 Subject Index. |
| Responsibility: | Lutz F. Tietze, Theophil Eicher, Ulf Diederichsen, Andreas Speicher. |
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"I thoroughly recommend this textbook for any of its target audience. It should be in every library ... And on the personal bookshelves of each of its intended readers as well... .An invaluable aid." (The Higher Education Academy Physical Sciences Centre, December 2008) "Recommended. Upper-division undergraduates through professionals." (CHOICE, April 2008) Read more...
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