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Solubilization and dispersion of carbon nanotubes

Author: Oxana Vasilievna Kharissova; Boris I Kharisov
Publisher: Cham, Switzerland : Springer, 2017 ©2017
Edition/Format:   eBook : Document : EnglishView all editions and formats
Summary:
This book describes a series of contemporary techniques and their combinations used for CNTs solubilization, from physical to chemical and biological, applying inorganic and organic compounds, as well as some metal complexes. In some cases, successive steps can be applied, for instance the use of low and high-weight surfactants, or mineral acid treatment for creation of -OH and -COOH groups and their further  Read more...
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Genre/Form: Electronic books
Additional Physical Format: Print version:
(OCoLC)992746647
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: Oxana Vasilievna Kharissova; Boris I Kharisov
ISBN: 9783319629506 3319629506
OCLC Number: 1003088055
Description: 1 online resource : illustrations
Contents: Preface; Contents; Authors; Chapter 1: Introduction; References; Chapter 2: Physical Methods; 2.1 Ultrasonication; 2.2 Plasma Treatment of CNTs; 2.3 Irradiation Techniques and Labeling; 2.4 Mechanical and Related Methods; 2.5 Pulsed Streamer Discharge; 2.6 Microwave Treatment; 2.7 Hydrothermal Method; 2.8 UV and Visible Light; 2.9 Other Physical Methods; References; Chapter 3: Chemical Methods; 3.1 Functionalization Leading to Soluble CNTs; 3.1.1 Inorganic Compounds; 3.1.1.1 Ozone; 3.1.1.2 Liquid Ammonia; 3.1.1.3 Inorganic Peroxides; 3.1.1.4 Elemental Metals; 3.1.1.5 Elemental Nonmetals. 3.1.1.6 CO2 and SiO2; 3.1.1.7 Inorganic Salts and Oxides; 3.1.1.8 Strong Acidic Media (Inorganic Acids and Their Mixtures); 3.1.2 Organic Compounds; 3.1.2.1 Aliphatic, Aromatic, and Polyaromatic Compounds; 3.1.2.2 Organic Acids, Their Salts, and Other Compounds Containing O-Containing Moieties; 3.1.2.3 Compounds with N-Containing Moieties; 3.1.2.4 Compounds with S-Containing Moieties; 3.1.2.5 Specific Organic Dispersants; 3.1.3 Coordination and Organometallic Compounds; 3.1.3.1 Solubilization of CNTs Hybrids with Metal Complexes of O-Containing Ligands. 3.1.3.2 Composites of CNTs with Metal Complexes of N-Containing Ligands; 3.1.3.3 Porphyrin- and Metalloporphyrin-Functionalized Carbon Nanotubes; 3.1.3.4 Composites of CNTs with Complexes of Sulfur-Containing Ligands; 3.1.3.5 Functionalization of CNTs with Organometallics and Grignard Reagents; 3.1.4 Polymers or Their Precursors; 3.1.5 Natural Products; 3.1.5.1 Inorganic Natural Products; 3.1.5.2 Organic Natural Products; References; Chapter 4: Biological/Biochemical Methods; 4.1 Sugars and Biomolecules; References; Chapter 5: Special Studies and Characterization of CNT Dispersions. 5.1 Dispersion, Precipitation, and Purification Studies; 5.1.1 Dispersion of CNTs in Solvents; 5.1.2 Precipitation of CNTs from Dispersions; 5.1.3 Comparison of Surfactant Abilities; 5.1.4 Combinations of Surfactants; 5.1.5 UV and Visible Light Influence; 5.1.6 Reactivity of Soluble CNTs Toward Active Oxygen Sources; 5.1.7 Selected Studies on Carboxylated and Amine-Functionalized CNTs; 5.1.8 Purification of Soluble CNTs; 5.1.9 Other Particular Studies; 5.2 Special Investigations on SWCNT Dispersion; 5.3 Dispersion of Different Types of CNTs (SWCNTs, DWCNTs, and MWCNTs). 5.4 Characterization of CNT Dispersions Within Solution; 5.4.1 UV-Visible Spectroscopy and Its Combinations; 5.4.2 Raman Spectroscopy and FTIR; 5.4.3 Small-Angle X-ray and Neutron Scattering; 5.4.4 SEM Studies; 5.4.5 TEM Studies; 5.4.6 AFM Studies; 5.4.7 Electrical Conductivity Measurements; 5.5 Toxicity of CNT Dispersions; References; Chapter 6: Cost and Main Applications of Soluble CNTs; References; Chapter 7: Training on CNT Solubilization; 7.1 Ultrasonication; 7.2 Plasma Treatment; 7.3 Shear Force Mixing; 7.4 Hydrothermal Method; 7.5 Ozonation.
Responsibility: Oxana Vasilievna Kharissova, Boris Ildusovich Kharisov.

Abstract:

This book describes a series of contemporary techniques and their combinations used for CNTs solubilization, from physical to chemical and biological, applying inorganic and organic compounds, as well as some metal complexes. In some cases, successive steps can be applied, for instance the use of low and high-weight surfactants, or mineral acid treatment for creation of -OH and -COOH groups and their further interaction with organic molecules. Each discussed method leads to an improvement of CNT solubility, frequently a considerable one. The formed dispersions can be stable for long periods of time, from several weeks to some months, and they sometimes even remain stable after centrifugation. Several special studies have been carried out in the areas of influence of solvent and light on CNTs dispersibility, combinations and abilities of surfactants, CNT cytotoxicity, etc. Applications of solubilized CNTs are discussed in this book as well.

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