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Spectrometric identification of organic compounds.

Author: Robert M Silverstein; Francis X Webster; David J Kiemle
Publisher: Hoboken, NJ : John Wiley & Sons, ©2005.
Edition/Format:   Print book : English : 7th ed.View all editions and formats
Database:WorldCat
Summary:

Originally published in 1962, this book explores the identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in  Read more...

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Genre/Form: Textbooks
Additional Physical Format: Online version:
Silverstein, Robert M. (Robert Milton), 1916-2007.
Spectrometric identification of organic compounds.
Hoboken, NJ : John Wiley & Sons, ©2005
(OCoLC)704439660
Material Type: Internet resource
Document Type: Book, Internet Resource
All Authors / Contributors: Robert M Silverstein; Francis X Webster; David J Kiemle
ISBN: 0471393622 9780471393627 0471429139 9780471429135
OCLC Number: 58546559
Description: x, 502 pages : illustrations ; 29 cm
Contents: Ch. 1. Mass spectrometry --
Ch. 2. Infrared spectrometry --
Ch. 3. Proton magnetic resonance spectrometry --
Ch. 4. Carbon-13 NMR spectrometry --
Ch. 5. Correlation NMR spectrometry; 2-D NMR --
Ch. 6. NMR spectrometry of other important spin 1/2 nuclei --
Ch. 7. Solved problems --
Ch. 8. Assigned problems.
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Table of Contents:

by clayton994 (WorldCat user on 2008-09-30)

Chapter 1. Mass Spectrometry -- 1.1 Introduction -- 1.2 Instrumentation -- 1.3 Ionization Methods -- 1.4 Mass Analyzers -- 1.5 Interpretation of El Mass Spectra -- 1.6 Mass Spectra of Some Chemical Classes -- Chapter 2. Infrared Spectrometry -- 2.1 Introduction -- 2.2 Theory -- 2.3 Instrumentation -- 2.4 Sample Handling -- 2.5 Interpretations of Spectra -- 2.6 Characteristic Group Absorption of Organic Molecules -- Chapter 3. Proton Magnetic Resonance Spectrometry -- 3.1 Introduction -- 3.2 Theory -- 3.3 Instrumentation and Sample Handling -- 3.4 Chemical Shift -- 3.5 Spin Coupling, Multiplets, Spin Systems -- 3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons -- 3.7 Coupling of Protons to Other Important Nuclei (F19, E, P31, Si29, and C13 -- 3.8 Chemical Shift Equivalence -- 3.9 Magnetic Equivalence (Spin-Coupling Equivalence) -- 3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants -- 3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling -- 3.12 Chirality -- 3.13 Vicinal and Geminal Coupling -- 3.14 Low-Range Coupling -- 3.15 Selective Spin Decoupling. Double Resonance -- 3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space -- Chapter 4. Carbon-13 NMR Spectrometry -- 4.1 Introduction -- 4.2 Theory -- 4.3 Interpretation of a Simple C13 Spectrum: Diethyl Phthalate -- 4.4 Quantitative C13 Analysis -- 4.5 Chemical Shift Equivalence -- 4.6 DEPT -- 4.7 Chemical Classes and Chemical Shifts -- Chapter 5. Correlation NMR Spectrometry; 2-D NMR -- 5.1 Introduction -- 5.2 Theory -- 5.3 Correlation Spectrometry -- 5.4 Ipsenol: H1-H1 COSY -- 5.5 Caryophyllene Oxide -- 5.6 C13-C13 Correlations: Inadequate -- 5.7 Lactose -- 5.8 Relayed Coherence Transfer: TOCSY -- 5.9 HMQC ? TOCSY -- 5.10 ROESY -- 5.11 VGSE -- 5.12 Gradient Field NMR -- Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei -- 6.1 Introduction -- 6.2 N15 Nuclear Magnetic Resonance -- 6.3 F19 Nuclear Magnetic Resonance -- 6.4 Si29 Nuclear Magnetic Resonance -- 6.5 P31 Nuclear Magnetic Resonance -- 6.6 Conclusion -- Chapter 7. Solved Problems -- 7.1 Introduction -- Chapter 8. Assigned Problems -- 8.1 Introduction -- Problems.

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