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Argonne National Lab

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Works: 13,762 works in 14,753 publications in 1 language and 57,509 library holdings
Roles: Researcher, Sponsor
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Publications about Argonne National Lab
Publications by Argonne National Lab
Most widely held works by Argonne National Lab
Automated tuning of the advanced photon source booster synchrotron ( Computer File )
23 editions published in 1997 in English and held by 92 libraries worldwide
The Advanced Photon Source (APS) consists of a linac, position accumulator ring (PAR), booster synchrotron, storage ring, and up to 70 experimental beamlines. The Access Control and Interlock System (ACIS) utilizes redundant programmable logic controllers (PLCs) and a third hard-wired chain to protect personnel from prompt radiation generated by the linac, PAR, synchrotron, and storage ring. This paper describes the ACIS's design philosophy, configuration, hardware, functionality, validation requirements, and operational experience
Effect of the Keck telescope's segmented primary on the performance on the Keck adaptive optics system ( Computer File )
8 editions published in 1997 in English and held by 32 libraries worldwide
XOP (X-ray OPtics utilities) is a graphical user interface (GUI) created to execute several computer programs that calculate the basic information needed by a synchrotron beamline scientist (designer or experimentalist). Typical examples of such calculations are: insertion device (undulator or wiggler) spectral and angular distributions, mirror and multilayer reflectivities, and crystal diffraction profiles. All programs are provided to the user under a unified GUI, which greatly simplifies their execution. The XOP optics applications (especially mirror calculations) take their basic input (optical constants, compound and mixture tables) from a flexible file-oriented database, which allows the users to select data from a large number of choices and also to customize their own data sets. XOP includes many mathematical and visualization capabilities. It also permits the combination of reflectivities from several mirrors and filters, and their effect, onto a source spectrum. This feature is very useful when calculating thermal load on a series of optical elements. The XOP interface is written in the IDL (Interactive Data Language). An embedded version of XOP, which freely runs under most Unix platforms (HP, Sun, Dec, Linux, etc) and under Windows95 and NT, is available upon request
Structure and dynamics of phosphate glasses From ultra- to orthophosphate composition ( Computer File )
7 editions published in 1997 in English and held by 28 libraries worldwide
Time-of-flight neutron powder diffraction studies of incrementally neutron-irradiated U₃Si and U₃Si₂ have revealed details of progressive amorphization of bulk materials, crystalline transformation prior to amorphization, elastic strain and diffuse scattering resulting from scattering interference between crystalline and amorphous fractions. Density differences between amorphous and crystalline fractions give rise, respectively, to tensile and compressive strain in U₃Si and U₃Si₂. Diffuse scattering associated with each Bragg peak shows crystallographic direction-dependent variation both in magnitude and displacement (relative to the Bragg position). A theoretical model describing this behavior relates the size of the amorphous zones, and the magnitude and displacement of the diffuse scattering contribution. After complete amorphization of U₃Si and U₃Si₂, anneals to progressively higher temperatures generate gradual evolution of the short- to intermediate-range amorphous structures prior to re-crystallization
Assessment results of the Indonesian TRIGA SNF to be shipped to INEEL ( Computer File )
6 editions published in 1997 in English and held by 24 libraries worldwide
Twelve different uranium alloys and compounds with uranium densities greater than 13.8 g/cc were fabricated into fuel plates. Sixty-four experimental fuel plates, referred to as microplates, with overall dimensions of 76.2 mm x 22.2 mm x 1.3 mm and elliptical fuel zone of nominal dimensions of 51 mm x 9.5 mm, began irradiation in the Advanced Test Reactor on August 23, 1997. The fuel test matrix consists of machined or comminuted (compositions are in weight %) U-10Mo, U-8Mo, U-6Mo, U-4Mo, U-9Nb-3Zr, U-6Nb-4Zr, U-5Nb-3Zr, U-6Mo-1Pt, U6Mo-0.6 Ru, U-10Mo-0.05Sn, U₂Mo and U₃Si₂ (as a control). The low enriched (²³⁵U <20%) fuel materials were cast, powdered, mixed with aluminum dispersant at a volume ratio of 1:3, compacted and hot rolled to form the microplates. Spherical atomized powders of two fuels, U-10Mo and U₃Si₂, were utilized to make microplates and included in the irradiation test as well. The experimental design and fabrication steps employed in the selection and production of the fueled microplates is discussed
Grout and vitrification formula development for immobilization of hazardous radioactive tank sludges at ORNL ( Computer File )
6 editions published in 1997 in English and held by 24 libraries worldwide
Utilization of adsorption on solid surfaces was exercised for the first time in 1785. Practical application of unactivated carbon filters, and powdered carbon were first demonstrated in the American water treatment plant, and a municipal treatment plant in New Jersey, in 1883 and 1930, respectively. The use of activated carbon became widespread in the next few decades. At present, adsorption on carbons has a wide spread application in water treatment and removal of taste, odor, removal of synthetic organic chemicals, color-forming organics, and desinfection by-products and their naturally occurring precursors. This paper presents an analysis of the surface fractal dimension and adsorption capacity of a group of carbons
Calibration of the stellar X-ray polarimeter ( Computer File )
5 editions published in 1997 in English and held by 20 libraries worldwide
X-ray optical elements (such as single-crystal silicon monochromators) illuminated with high-power synchrotron-radiation beams produced by insertion devices and, to a lesser extent bending magnets, require cooling, When operating a silicon crystal at room temperature, channels for the coolant are often fabricated directly beneath the diffracting surface. Then a separate silicon distribution manifold/plenum is manufactured, and the components are bonded together using an adhesive or some intermediate material. In many cases, such monochromators suffer from strains induced by the bond. A silicon-to-silicon direct-bonding technique (i.e., without any intermediate material) has been developed that appears to be an attractive method for creating a bond with less strain between two pieces of silicon. This technique is well understood for the case of thin wafers ((approximately)0.5 mm thickness) and is used by the semiconductor industry. Recently, bonding of 16-mm-thick 10-cm-diameter silicon crystals has been successfully performed inducing very little strain. A short review of the silicon-to-silicon crystals has been successfully performed inducing very little strain. A short review of the silicon-to-silicon direct-bonding process will be presented with an emphasis on its application to room temperature high-heat-load x-ray optics with the present status of direct bonding efforts at the APS
Risk analyses for disposing of nonhazardous oil field wastes in salt caverns ( Computer File )
5 editions published in 1997 in English and held by 20 libraries worldwide
The exploration and production segment of the U.S. oil and gas industry generates millions of barrels of nonhazardous oil field wastes annually. In most cases, operators can dispose of their oil fields wastes at a lower cost on-site than off site and, thus, will choose on-site disposal. However, a significant quantity of oil field wastes are still sent to off-site commercial facilities for disposal. This paper provides information on the availability of commercial disposal companies in different states, the treatment and disposal methods they employ, and how much they charge. There appear to be two major off-site disposal trends. Numerous commercial disposal companies that handle oil field wastes exclusively are located in nine oil-and gas-producing states. They use the same disposal methods as those used for on-site disposal. In addition, the Railroad Commission of Texas has issued permits to allow several salt caverns to be used for disposal of oil field wastes. Twenty-two other oil- and gas-producing states contain few or no disposal companies dedicated to oil and gas industry waste. The only off-site commercial disposal companies available handle general industrial wastes or are sanitary landfills. In those states, operators needing to dispose of oil field wastes off-site must send them to a local landfill or out of state. The cost of off-site commercial disposal varies substantially, depending on the disposal method used, the state in which the disposal company is located, and the degree of competition in the area
Plastic flow in fcc metals induced by single-ion impacts ( Computer File )
4 editions published in 1997 in English and held by 16 libraries worldwide
Irradiation of Au and Pb foils with Xe ions at temperatures between 30 and 450 K has been monitored using in-situ transmission electron microscopy. Single ion impacts give rise to surface craters on the irradiated surface with sizes as large as 12 nm. Approximately 2--5% of impinging ions produce craters on Au while only about 0.6% produce craters on Pb. Larger craters on Au frequently have expelled material associated with them. Temporal details of crater formation and annihilation has been recorded on video with a time resolution of 33 milliseconds. Craters annihilate in discrete steps due to subsequent ion impacts or anneal in a continuous manner due to surface diffusion. Craters production (those persisting for one or more video frames) as a function of temperature indicates that the surface diffusion process responsible for thermal annealing of craters has an activation energy of 0.76 eV in Au. Crater creation results from plastic flow associated with near surface cascades. Crater annihilation in discrete steps results from plastic flow induced by subsequent ion impacts, including those that do not themselves produce a crater
The U.S. DOE MPC and A assistance program to Ukraine ( Computer File )
4 editions published in 1997 in English and held by 16 libraries worldwide
This paper, augmented by color slides and handouts, will examine the inherent security benefits of underground dry storage of nuclear materials. Specific items to be presented include: the successful implementation of this type of storage configuration at Argonne National Laboratory - West; facility design concepts with security as a primary consideration; physical barriers achieved by container design; detection, assessment, and monitoring capabilities; and {open_quotes}self protection{close_quotes} strategies. This is a report on the security features of such a facility. The technical operational aspects of the facility are beyond the scope of this paper
Construction of filter vectors for the information-efficient spectral imaging sensor ( Computer File )
4 editions published in 1998 in English and held by 16 libraries worldwide
XOP (X-ray OPtics utilities) is a graphical user interface (GUI) to run computer programs which calculate basic information needed by synchrotron radiation beamline scientists and engineers. It can also be used as a front-end for specific codes or packages for data analysis and data reduction (XAFS, surface crystallography, etc.). XOP contains a customized database for optical and atomic constants. It has a flexible design and new applications may be added. The capabilities of XOP including those related to simulations of crystal diffraction profiles and multilayer reflectivities are summarized. The authors discuss the most recent developments which have been included in the XOP version 2.0. A few other examples of typical calculations are: insertion device (undulator and wiggler) spectra and angular distributions, mirror and multilayer reflectivities, and crystal diffraction profiles. The computer programs are executed and the results are analyzed within the GUI which make them fast and easy to use. The XOP interface is written in the Interactive Data Language (IDL) from Research Systems Inc., and it runs on the Unix (HP, Sun, Linux, DEC-Alpha, and Silicon Graphics), and on the Windows 95/NT operating systems. It has been built with an IDL license embedded and is available under some limited conditions free of charge from the authors
Performance Modeling Applied to the Treatment and Disposal of a Mixed Waste at the SRS ( Computer File )
4 editions published in 1997 in English and held by 16 libraries worldwide
The U.S. Department of Energy supports an applied superconductivity program entitled {open_quotes}Superconductivity Program for Electric Power Systems.{close_quotes} Activities under this program are designed to help develop the high-temperature superconductor (HTS) technology that is needed for industry to proceed with the commercial development of electric power applications. Research is conducted in three categories: wire development, systems technology development, and Superconductivity Partnership Initiative (SPI). Wire development activities are devoted to improving the critical current density (J{sub c}) of short-length HTS wire, whereas activities in systems technology development focus on fabrication of long-length wires, coils, and magnets. Finally, SPI activities focus on the development of prototypes that consist of a generator coil, a fault current limiter, a transmission cable, and a motor. A current overview and recent progress in the development of HTSs are outlined in this paper. 48 refs., 6 figs
The RERTR Program a status report ( Computer File )
4 editions published between 1991 and 1998 in English and held by 16 libraries worldwide
The progress of the Reduced Enrichment Research and Test Reactor (RERTR) Program is described. The major events, findings, and activities of 1991 are reviewed after a brief summary of the results which the RERTR Program had achieved by the end of 1990 in collaboration with its many international partners
Measurement of diffraction gratings with a long trace profiler with applications for synchrotron beamline gratings ( Computer File )
4 editions published in 1997 in English and held by 16 libraries worldwide
We have tested the first diamond double-crystal monochromator at the Advanced Photon Source (APS). The monochromator consisted of two synthetic type lb (111) diamond plates in symmetric Bragg geometry. We tested two pairs of single-crystal plates: the first pair was 6 mm by 5 mm by 0.25 mm and 6 mm by 5 mm by 0.37 mm; the second set was 7 mm by 5.5 mm by 0.44 mm. The monochromator first crystal was indirectly cooled by edge contact with a water-cooled copper holder. We studied the performance of the monochromator under the high-power x-ray beam delivered by the APS undulator A. We found no indication of thermal distortions or strains even at the highest incident power (280 watts) and power density (123 W/mm² at normal incidence). The calculated maximum power and power density absorbed by the first crystal were 37 watts and 16 W/mm² respectively. We also compared the maximum intensity delivered by the diamond monochromator and by a silicon (111) cryogenically cooled monochromator. For energies in the range of 6 to 10 keV, the flux through the diamond monochromator was about a factor of two less than through the silicon monochromator, in good agreement with calculations. We conclude that water-cooled diamond monochromators can handle the high-power beams from the undulator beams from the undulator beamlines at the APS. As single-crystal diamond plates of larger size and better quality become available, the use of diamond monochromators will become a very attractive option
Relationship between fabrication parameters and structural characteristics of sintered lithium orthosilicate ( Computer File )
4 editions published in 1988 in English and held by 13 libraries worldwide
Lithium orthosilicate (Li₄SiO₄) powder was synthesized by the solid-state reaction of lithium oxide with amorphous silica, and the effects of fabrication parameters on the structural characteristics of the product were investigated. Processing considerations such as milling media, drying technique, calcination time and temperature, pressing behavior, sintering time and temperatures, and impurity concentration were addressed. The initial powder particle size was observed to be important in achieving high sintered density, with densities as high as 98% TD achieved with a particle size of approximately 1 ..mu..m. 9 refs., 6 figs
Phase loop bandwidth measurements on the advanced photon source 352 MHz rf systems ( Computer File )
3 editions published in 1997 in English and held by 12 libraries worldwide
A switching control system has been designed and built to provide the capability of rapidly switching the waveguide and low-level cabling between different klystrons to operate the Advanced Photon Source storage ring in the event of a failure of a klystron system or to perform necessary repairs and preventative maintenance. The twelve possible modes of operation allow for complete redundancy of the booster synchrotron rf system and either a maximum of two storage ring rf systems to be completely off-line or one system to be used as a power source for an rf test stand. A programmable controller is used to send commands to intermediate control panels which interface to WR2300 waveguide switches and phase shifters, rf cavity interlock and low-level rf distribution systems, and klystron power supply controls for rapid reconfiguration of the rf systems in response to a mode-selection command. Mode selection is a local manual operation using a keyswitch arrangement which prevents more than one mode from being selected at a time. The programmable controller also monitors for hardware malfunction and guards against {open_quotes}hot-switching{close_quotes} of the rf systems. The rf switching controls system is monitored via the Experimental Physics and Industrial Control System (EPICS) for remote system status check
Diamond monochromator for high heat flux synchrotron x-ray beams ( file )
3 editions published between 1992 and 1993 in English and held by 12 libraries worldwide
Single crystal silicon has been the material of choice for x-ray monochromators for the past several decades. However, the need for suitable monochromators to handle the high heat load of the next generation synchrotron x-ray beams on the one hand and the rapid and on-going advances in synthetic diamond technology on the other make a compelling case for the consideration of a diamond mollochromator system. In this Paper, we consider various aspects, advantage and disadvantages, and promises and pitfalls of such a system and evaluate the comparative an monochromator subjected to the high heat load of the most powerful x-ray beam that will become available in the next few years. The results of experiments performed to evaluate the diffraction properties of a currently available synthetic single crystal diamond are also presented. Fabrication of diamond-based monochromator is within present technical means
Problem decomposition and domain-based parallelism via group theoretic principles ( Computer File )
3 editions published in 1997 in English and held by 12 libraries worldwide
This paper provides an overview of coupled reactor physics and thermal-hydraulics computations with the SAS-DIF3DK computer code. The assumptions and capabilities of the DIF3D-K nodal diffusion theory spatial kinetics model are presented. Results from DIF3D-K benchmark verification calculations are reported. SAS thermal-hydraulics model assumptions and features are described, and results from a prototypic application are shown. The details of data flow in the coupling of spatial kinetics with thermal-hydraulics are reviewed, and coupled applications are described. Future model developments are listed
MOCVD capacitors ( Computer File )
3 editions published in 1997 in English and held by 12 libraries worldwide
A significant effort within the Department of Energy's Office of Transportation Technologies and the U.S. Navy's Power Electronic Building Block (PEBB) project has focused on reducing the size and weight of power electronic devices for electric and hybrid vehicles. Power electronic circuits, which are composed of active switching elements and passive components such as capacitors and inductors, provide motor control, power distribution, and DC/AC conversion functions in electric vehicles. Progress has been made on reducing the size and weight of power electronic components such as MOS-controlled thristors and insulated-gate bipolar transistors. Additional effort on high-power capacitors will be needed for load leveling and filter functions. The objective of this work is to fabricate a new class of high-power capacitors with reduced size and weight. Capacitors will be integrated with semiconductor components of electric motor and actuator control subsystems
Noise control of radiological monitoring equipment ( Computer File )
3 editions published in 1998 in English and held by 12 libraries worldwide
Argonne National Laboratory West (ANL-W) is verifying the characterization and repackaging of contact-handled transuranic (CH-TRU) mixed waste in support of the Waste Isolation Pilot Program (WIPP) project located in Carlsbad, New Mexico. The WIPP Waste Characterization Chamber (WCC) was designed to allow opening of transuranic waste drums for this process. The WCC became operational in March of 1994 and has characterized approximately 240 drums of transuranic waste. The waste drums are internally contaminated with high levels of transuranic radionuclides. Attaching and detaching drums to the glove box posed serious contamination control problems. Prior to characterizing waste, several drum attachment techniques and materials were evaluated. An inexpensive HEPA filter molded into the bagging material helps with venting during detachment. The current techniques and procedures used to attach and detach transuranic waste drums to the WCC are described
Compensation for the effect of vacuum chamber eddy current by digital signal processing for closed orbit feedback ( file )
3 editions published in 1993 in English and held by 12 libraries worldwide
The Advanced Photon Source (APS) will implement both global and local beam position feedback systems to stabilize the particle and X-ray beams. The relatively thick (1/2 inch) aluminum storage ring vacuum chamber at corrector magnet locations for the local feedback systems will induce significant eddy current. This will reduce the correction bandwidth and could potentially destabilize the feedback systems. This paper describes measurement of the effect of the eddy current induced in the APS storage ring vacuum chamber by a horizontal/vertical corrector magnet and its compensation using digital signal processing at 4 kHz sampling frequency with proportional, integral, and derivative (PID) control algorithm for closed orbit feedback. A theory of digital feedback to obtain the linear system responses and the conditions for optimal control will also be presented. The magnet field in the vacuum chamber shows strong quadrupole and sextupole components varying with frequency, in addition to significant attenuation and phase shift with bandwidth ( -3 dB) of 20 Hz for horizontal and 4 Hz for vertical fields relative to the magnet current. Large changes in the magnet resistance and inductance were also observed, as the result of reduced total magnetic energy and increased Ohmic heat loss
 
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