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Advances in chemistry research. Volume 50

Author: James C Taylor
Publisher: New York : Nova Science Publishers, [2019]
Edition/Format:   eBook : Document : English
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Genre/Form: Electronic books
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: James C Taylor
ISBN: 9781536148084 1536148083
OCLC Number: 1085348654
Description: 1 online resource
Contents: Intro; Contents; Preface; Chapter 1; Selected Aspects of the Analytical Chemistry of Amlodipine, a Widely Used Long Acting Calcium Antagonist; Abstract; Introduction; Synthesis and Characterization. The Drug and Its Impurities; Synthesis of Amlodipine; Amlodipine and Its Salts; Amlodipine in the Pharmacopeias. Official Status; Chemical Sources of the Official Impurities of the EP7; Synthesis of Some Official Impurities of the EP7; Impurity Profiling of Amlodipine Besylate; Mass Spectrometric Analyses: Impurities and Metabolites; Genotoxic Impurities; Stability of Amlodipine Thermal StabilityAcid-Base Degradation; Photostability; Stability in Solid and Liquid Formulations; Compatibility with Other Drugs and Excipients. Incompatibilities; Stability Indicating Assays; Amlodipine as a Chiral Drug. Preparation, Separation, Quantitation, Metabolism; Phase Transformations; Acknowledgments; References; Chapter 2; Numerical Simulations of the Effect of Flow Path Geometric Features on Chemical Reactions in Compressible Flow; Abstract; 1. Introduction; 1.1. Background; 1.2. Scope of the Work; 2. Theory; 2.1. Equation of State and Gas Properties 2.1.1. Pure Gas Species Properties2.1.2. Gas Mixture Properties; 2.1.3. Chemical Reactions; 2.1.4. Governing Differential Equations; 2.2. Computational Methods; 2.3. Problem Statement; 3. Results; 3.1. Configuration A --
Straight; 3.2. Configuration B --
Constrict; 3.3. Configuration C --
Straight-Rough; 3.4. Configuration D --
Straight-Bleed; 3.5. Configuration E --
Expansion; 3.6. Configuration F --
Expansion with Filter; 3.7. Configuration G --
Expansion with Baffles; 3.8. Configuration H --
Expansion with Roughness; 3.9. Configuration I --
Expansion with Obstruction; 4. Discussion; Conclusion AppendixReferences; Chapter 3; Carbonylation Reactions: Impacts of Homogeneous and Heterogeneous Catalysts and Carbon Monoxide Surrogates; Abstract; Introduction; Homogeneous Carbonylation Reactions; Carbonylation of Methanol to Produce Acetic Acid; Industrial Processes; The Cobalt-Based BASF Process; The Rhodium-Based Monsanto Process; The Iridium-Based Cativa Process of BP Chemicals; Laboratory Processes; Different Processes for Carbonylation of Methanol to Produce Acetic Acid; Nickel-Complex Catalyst; Ligand Based Metal-Complexes; Phosphine-Based Ligands Promoters Rhodium-Nitrogen and Nitrogen-Oxygen Based Ligands Complexes as PromotorsIridium Carbonyl Complexes of Nitrogen and Nitrogen-Oxygen Donor Ligands as Promoters; Heterogeneous Catalysts for Carbonylation of Methanol; Other Carbonylation Reactions; Carbonylation of Diazo Group; Ortho-Acylation of Pyridine through Carbonylation; Carbonylation of 2-Nitro-N-(Phenyhnethylene) Benzeneamine; Carbonylation of Alkynes; Pauson-Khand Reaction (PKR); Carbonylation of Epoxides; CO Surrogates; Mo(CO)6 Promoted Carbonylations; Formic Acid (HCOOH) Promoted Carbonylations
Responsibility: James C. Taylor, editor.

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