skip to content
Design of the Extraction Process for Characterization of Volatile Profile of Stem Wood by Solid-Phase Microextraction Preview this item
ClosePreview this item
Checking...

Design of the Extraction Process for Characterization of Volatile Profile of Stem Wood by Solid-Phase Microextraction

Author: Bajer, Tomáš; Šulc, Jakub; Ventura, Karel; Bajerová, Petra
Publisher: SAGE PUBLICATIONS INC 2020-03-19T12:52:03Z 2020-03-19T12:52:03Z 2019
Edition/Format:   Downloadable archival material : English
Summary:
A method for isolation of volatile compounds from samples of stem wood by solid-phase microextraction was developed. The extraction method was optimized using a central composite design approach. Extraction temperature and extraction time were optimized in the ranges of 40 degrees C to 120 degrees C and 10 to 90 minutes, respectively. Final extraction method was combined with GC-MS for separation and identification
Rating:

(not yet rated) 0 with reviews - Be the first.

Subjects
More like this

Find a copy in the library

&AllPage.SpinnerRetrieving; Finding libraries that hold this item...

Details

Genre/Form: article
Document Type: Archival Material
All Authors / Contributors: Bajer, Tomáš; Šulc, Jakub; Ventura, Karel; Bajerová, Petra
OCLC Number: 1182629469
Language Note: English
Notes: p. nestránkováno
application/pdf
Other Titles: Návrh extrakčního procesu pro charakterizaci profilu těkavých látek dřeva s využitím mikroextrakce tuhou fází

Abstract:

A method for isolation of volatile compounds from samples of stem wood by solid-phase microextraction was developed. The extraction method was optimized using a central composite design approach. Extraction temperature and extraction time were optimized in the ranges of 40 degrees C to 120 degrees C and 10 to 90 minutes, respectively. Final extraction method was combined with GC-MS for separation and identification of volatile components of wood samples of seven tree species, commonly occurring in Central Europe. All of them were deciduous (acacia, alder, beech, elm, larch, maple, and oak). In total 185 organic compounds were identified in volatile profiles of all the samples by the developed method. To facilitate the evaluation of the suitability of the proposed method for extraction of different compound types, all identified compounds were categorized into 16 groups. Percentage of compound groups in volatile profiles of individual wood samples shows that the developed method is suitable for evaluation of a wide range of volatile components from stem wood.

Byl vyvinut způsob izolace těkavých sloučenin ze vzorků dřeva mikroextrakcí tuhou fází. Extrakce byla optimalizována pomocí metody centrálního kompozitního designu. Extrakční teplota a doba extrakce byly optimalizovány v rozmezí 40 °C až 120 °C a 10 až 90 minut. Optimalizovaná metoda extrakce byla spojena s GC-MS pro separaci a identifikaci těkavých složek vzorků dřeva sedmi druhů dřevin, které se běžně vyskytují ve střední Evropě (akácie, olše, buk, jilm, modřín, javor a dub). V profilech těkavých látek všech testovaných vzorků bylo identifikováno celkem 185 organických sloučenin. Pro usnadnění vyhodnocení vhodnosti navrhovaného způsobu extrakce různých typů sloučenin byly všechny identifikované sloučeniny roztříděny do 16 skupin. Procentuální podíl skupin sloučenin v těkavých profilech jednotlivých vzorků dřeva ukazuje, že vyvinutá metoda je vhodná pro hodnocení širokého spektra těkavých složek uvolňovaných z různých druhů dřeva.

Reviews

User-contributed reviews
Retrieving GoodReads reviews...
Retrieving DOGObooks reviews...

Tags

Be the first.
Confirm this request

You may have already requested this item. Please select Ok if you would like to proceed with this request anyway.

Linked Data


\n\n

Primary Entity<\/h3>\n
<http:\/\/www.worldcat.org\/oclc\/1182629469<\/a>> # Design of the Extraction Process for Characterization of Volatile Profile of Stem Wood by Solid-Phase Microextraction<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nlibrary:ArchiveMaterial<\/a>, schema:MediaObject<\/a>, schema:CreativeWork<\/a> ;\u00A0\u00A0\u00A0\nlibrary:oclcnum<\/a> \"1182629469<\/span>\" ;\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/drevo<\/a>> ; # d\u0159evo<\/span>\n\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/conifer<\/a>> ; # conifer<\/span>\n\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/broadleaf<\/a>> ; # broadleaf<\/span>\n\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/spme<\/a>> ; # SPME<\/span>\n\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/tekave_organicke_slouceniny<\/a>> ; # t\u011Bkav\u00E9 organick\u00E9 slou\u010Deniny<\/span>\n\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/wood<\/a>> ; # wood<\/span>\n\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/listnate_stromy<\/a>> ; # listnat\u00E9 stromy<\/span>\n\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/volatile_organic_compounds<\/a>> ; # volatile organic compounds<\/span>\n\u00A0\u00A0\u00A0\nschema:alternateName<\/a> \"N\u00E1vrh extrak\u010Dn\u00EDho procesu pro charakterizaci profilu t\u011Bkav\u00FDch l\u00E1tek d\u0159eva s vyu\u017Eit\u00EDm mikroextrakce tuhou f\u00E1z\u00ED<\/span>\" ;\u00A0\u00A0\u00A0\nschema:creator<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/bajer_tomas<\/a>> ; # Bajer, Tom\u00E1\u0161<\/span>\n\u00A0\u00A0\u00A0\nschema:creator<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/bajerova_petra<\/a>> ; # Bajerov\u00E1, Petra<\/span>\n\u00A0\u00A0\u00A0\nschema:creator<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/sulc_jakub<\/a>> ; # \u0160ulc, Jakub<\/span>\n\u00A0\u00A0\u00A0\nschema:creator<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/ventura_karel<\/a>> ; # Ventura, Karel<\/span>\n\u00A0\u00A0\u00A0\nschema:datePublished<\/a> \"2020\/03\/19T12:52:03Z<\/span>\" ;\u00A0\u00A0\u00A0\nschema:datePublished<\/a> \"2020<\/span>\" ;\u00A0\u00A0\u00A0\nschema:datePublished<\/a> \"2019<\/span>\" ;\u00A0\u00A0\u00A0\nschema:description<\/a> \"A method for isolation of volatile compounds from samples of stem wood by solid-phase microextraction was developed. The extraction method was optimized using a central composite design approach. Extraction temperature and extraction time were optimized in the ranges of 40 degrees C to 120 degrees C and 10 to 90 minutes, respectively. Final extraction method was combined with GC-MS for separation and identification of volatile components of wood samples of seven tree species, commonly occurring in Central Europe. All of them were deciduous (acacia, alder, beech, elm, larch, maple, and oak). In total 185 organic compounds were identified in volatile profiles of all the samples by the developed method. To facilitate the evaluation of the suitability of the proposed method for extraction of different compound types, all identified compounds were categorized into 16 groups. Percentage of compound groups in volatile profiles of individual wood samples shows that the developed method is suitable for evaluation of a wide range of volatile components from stem wood.<\/span>\" ;\u00A0\u00A0\u00A0\nschema:description<\/a> \"Byl vyvinut zp\u016Fsob izolace t\u011Bkav\u00FDch slou\u010Denin ze vzork\u016F d\u0159eva mikroextrakc\u00ED tuhou f\u00E1z\u00ED. Extrakce byla optimalizov\u00E1na pomoc\u00ED metody centr\u00E1ln\u00EDho kompozitn\u00EDho designu. Extrak\u010Dn\u00ED teplota a doba extrakce byly optimalizov\u00E1ny v rozmez\u00ED 40 \u00B0C a\u017E 120 \u00B0C a 10 a\u017E 90 minut. Optimalizovan\u00E1 metoda extrakce byla spojena s GC-MS pro separaci a identifikaci t\u011Bkav\u00FDch slo\u017Eek vzork\u016F d\u0159eva sedmi druh\u016F d\u0159evin, kter\u00E9 se b\u011B\u017En\u011B vyskytuj\u00ED ve st\u0159edn\u00ED Evrop\u011B (ak\u00E1cie, ol\u0161e, buk, jilm, mod\u0159\u00EDn, javor a dub). V profilech t\u011Bkav\u00FDch l\u00E1tek v\u0161ech testovan\u00FDch vzork\u016F bylo identifikov\u00E1no celkem 185 organick\u00FDch slou\u010Denin. Pro usnadn\u011Bn\u00ED vyhodnocen\u00ED vhodnosti navrhovan\u00E9ho zp\u016Fsobu extrakce r\u016Fzn\u00FDch typ\u016F slou\u010Denin byly v\u0161echny identifikovan\u00E9 slou\u010Deniny rozt\u0159\u00EDd\u011Bny do 16 skupin. Procentu\u00E1ln\u00ED pod\u00EDl skupin slou\u010Denin v t\u011Bkav\u00FDch profilech jednotliv\u00FDch vzork\u016F d\u0159eva ukazuje, \u017Ee vyvinut\u00E1 metoda je vhodn\u00E1 pro hodnocen\u00ED \u0161irok\u00E9ho spektra t\u011Bkav\u00FDch slo\u017Eek uvol\u0148ovan\u00FDch z r\u016Fzn\u00FDch druh\u016F d\u0159eva.<\/span>\" ;\u00A0\u00A0\u00A0\nschema:exampleOfWork<\/a> <http:\/\/worldcat.org\/entity\/work\/id\/10397367794<\/a>> ;\u00A0\u00A0\u00A0\nschema:genre<\/a> \"article<\/span>\" ;\u00A0\u00A0\u00A0\nschema:inLanguage<\/a> \"en<\/span>\" ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"Design of the Extraction Process for Characterization of Volatile Profile of Stem Wood by Solid-Phase Microextraction<\/span>\" ;\u00A0\u00A0\u00A0\nschema:productID<\/a> \"1182629469<\/span>\" ;\u00A0\u00A0\u00A0\nschema:publication<\/a> <http:\/\/www.worldcat.org\/title\/-\/oclc\/1182629469#PublicationEvent\/sage_publications_inc_2020_03_19t12_52_03z_2020_03_19t12_52_03z_2019<\/a>> ;\u00A0\u00A0\u00A0\nschema:publisher<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/sage_publications_inc<\/a>> ; # SAGE PUBLICATIONS INC<\/span>\n\u00A0\u00A0\u00A0\nwdrs:describedby<\/a> <http:\/\/www.worldcat.org\/title\/-\/oclc\/1182629469<\/a>> ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n\n

Related Entities<\/h3>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/bajer_tomas<\/a>> # Bajer, Tom\u00E1\u0161<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nbgn:Agent<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"Bajer, Tom\u00E1\u0161<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/bajerova_petra<\/a>> # Bajerov\u00E1, Petra<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nbgn:Agent<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"Bajerov\u00E1, Petra<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/sage_publications_inc<\/a>> # SAGE PUBLICATIONS INC<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nbgn:Agent<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"SAGE PUBLICATIONS INC<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/sulc_jakub<\/a>> # \u0160ulc, Jakub<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nbgn:Agent<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"\u0160ulc, Jakub<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/ventura_karel<\/a>> # Ventura, Karel<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nbgn:Agent<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"Ventura, Karel<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/broadleaf<\/a>> # broadleaf<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"broadleaf<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/conifer<\/a>> # conifer<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"conifer<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/drevo<\/a>> # d\u0159evo<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"d\u0159evo<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/listnate_stromy<\/a>> # listnat\u00E9 stromy<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"listnat\u00E9 stromy<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/spme<\/a>> # SPME<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"SPME<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/tekave_organicke_slouceniny<\/a>> # t\u011Bkav\u00E9 organick\u00E9 slou\u010Deniny<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"t\u011Bkav\u00E9 organick\u00E9 slou\u010Deniny<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/volatile_organic_compounds<\/a>> # volatile organic compounds<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"volatile organic compounds<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Thing\/wood<\/a>> # wood<\/span>\n\u00A0\u00A0\u00A0\u00A0a \nschema:Thing<\/a> ;\u00A0\u00A0\u00A0\nschema:name<\/a> \"wood<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/www.worldcat.org\/title\/-\/oclc\/1182629469<\/a>>\u00A0\u00A0\u00A0\u00A0a \ngenont:InformationResource<\/a>, genont:ContentTypeGenericResource<\/a> ;\u00A0\u00A0\u00A0\nschema:about<\/a> <http:\/\/www.worldcat.org\/oclc\/1182629469<\/a>> ; # Design of the Extraction Process for Characterization of Volatile Profile of Stem Wood by Solid-Phase Microextraction<\/span>\n\u00A0\u00A0\u00A0\nschema:dateModified<\/a> \"2020-08-06<\/span>\" ;\u00A0\u00A0\u00A0\nvoid:inDataset<\/a> <http:\/\/purl.oclc.org\/dataset\/WorldCat<\/a>> ;\u00A0\u00A0\u00A0\nvoid:inDataset<\/a> <http:\/\/purl.oclc.org\/dataset\/WorldCat\/DigitalCollectionGateway<\/a>> ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n
<http:\/\/www.worldcat.org\/title\/-\/oclc\/1182629469#PublicationEvent\/sage_publications_inc_2020_03_19t12_52_03z_2020_03_19t12_52_03z_2019<\/a>>\u00A0\u00A0\u00A0\u00A0a \nschema:PublicationEvent<\/a> ;\u00A0\u00A0\u00A0\nschema:organizer<\/a> <http:\/\/experiment.worldcat.org\/entity\/work\/data\/10397367794#Agent\/sage_publications_inc<\/a>> ; # SAGE PUBLICATIONS INC<\/span>\n\u00A0\u00A0\u00A0\nschema:startDate<\/a> \"2019<\/span>\" ;\u00A0\u00A0\u00A0\nschema:startDate<\/a> \"2020-03-19T12:52:03Z<\/span>\" ;\u00A0\u00A0\u00A0\u00A0.\n\n\n<\/div>\n\n

Content-negotiable representations<\/p>\n