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Mass Spectrometry.

Author: James M Thompson
Publisher: Milton : Pan Stanford Publishing, 2017.
Edition/Format:   eBook : Document : EnglishView all editions and formats
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Genre/Form: Electronic books
Additional Physical Format: Print version:
Thompson, James M.
Mass Spectrometry.
Milton : Pan Stanford Publishing, ©2017
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: James M Thompson
ISBN: 9781351207133 135120713X 9781351207140 1351207148
OCLC Number: 1019656455
Description: 1 online resource (163 pages)
Contents: Intro --
Halftitle --
Title Page --
Copyright page --
Table of Contents --
Preface --
Acknowledgments --
1 Some Fundamentals of Mass Spectrometry --
1.1 Introduction --
1.2 The Mass Spectrometer --
1.2.1 The Magnetic Sector Mass Spectrometer --
1.2.2 The Quadrupole Mass Spectrometer --
1.2.3 The Time-of-Flight Mass Spectrometer --
1.3 The Mass Spectrum --
1.3.1 Ion Fragments --
1.3.2 The Base Peak --
1.3.3 The Molecular or Parent Ion (M+) --
1.3.4 The (M + 1)+ Ion --
1.3.5 Isotopic Fragments --
1.3.6 High-Resolution Mass Spectrometry --
1.4 Depicting Mass Spectral Data --
1.5 The Molecular or Parent Ion --
1.6 Predicting the Formation of m+ --
1.7 The Nitrogen Rule --
1.8 Metastable Ions --
1.9 Doubly Charged Ions --
1.10 The General Fragmentation Process --
1.11 The Fragmentation of a Hypothetical Molecule --
1.12 Identifying the Molecular Ion --
1.13 Chemical Ionization --
1.14 High-Molecular-Weight Impurities --
1.15 The Fragmentation of M+ --
1.16 Determining the Molecular Ion from the Fragments --
1.17 Determining the Molecular Ion by Derivatization --
1.18 Determining M+ From Rates of Effusion --
1.19 General Rearrangement --
1.20 Skeletal Rearrangement --
1.21 The McLafferty Rearrangement --
1.22 The Loss of Neutral Fragments --
1.23 Atomic Weight Determinations --
1.24 The Isotopes of Carbon --
1.25 Calculating Relative Intensities --
1.26 The Experimental Determination of the Carbon Number --
1.27 Compounds Containing Bromine and/or Chlorine --
1.28 Compounds Containing Sulfur --
1.29 Beynon's Table --
1.30 Some Techniques, Innovations, and Applications in Mass Spectrometry --
1.30.1 Thermogravimetric Analysis-Mass Spectrometry (TG/MS) and Thermogravimetric Analysis-Fourier Transform Infrared (TG/FTIR) --
1.30.2 TG/MS Systems --
1.30.3 The TG/MS Interface --
1.30.4 TG/MS Data Collecting and Processing Software. 1.30.5 GC/MS, GC/FTIR and GC/MS/FTIR --
1.30.6 The GC/MS and GC/FTIR and GC/MS/FTIR Interfaces --
2 The Analysis of Mass Spectra --
2.1 The Fragmentation Patterns of Straight-Chain Alkanes --
2.2 Branched Alkanes --
2.3 Cycloalkanes --
2.4 Unsaturated Hydrocarbons --
2.5 Alkyl Halides --
2.6 Phenyl Halides --
2.7 Benzyl Halides --
2.8 Aliphatic Ethers --
2.9 Alcohols --
2.10 Phenols --
2.11 Aliphatic Ketones --
2.12 Aromatic Ketones --
2.13 Aliphatic Aldehydes --
2.14 Aromatic Aldehydes --
2.15 Anhydrides --
2.16 Acetals and Ketals --
2.17 Aliphatic Acids --
2.18 Aromatic Acids --
2.19 Aliphatic Amines --
2.20 Aromatic Amines --
2.21 Amides --
2.22 Aliphatic Nitro Compounds --
2.23 Aromatic Nitro Compounds --
3 Problems in Mass Spectrometry --
3.1 Introduction --
3.2 Some General Suggestions for Interpreting Mass Spectra --
3.3 Criteria for Finding the Molecular Ion --
3.4 Interpretation of a Mass Spectrum Using the National Institute of Standards and Technology (NIST) Mass Spectral Search Program --
3.5 Problems --
3.6 On the Stability of Molecules --
3.6.1 Complex Molecules Revisited --
3.7 On Detecting Iodine in the Molecule --
3.8 More on Non-Branched Hydrocarbons --
3.9 On the Loss of Fragments from the Molecular Ion --
3.9.1 Loss of H --
3.10 Loss of a methyl group --
3.11 Loss of HF from the Molecular Ion --
3.12 On the Loss of Water from Alcohols --
Suggested Readings and References --
Appendix --
A.1 Graphic Presentation of Isotopic Peaks --
A.2 Silicon and Sulfur Isotopic Peaks --
Index.

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