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Measuring Elemental Impurities in Pharmaceuticals : a Practical Guide

Author: Robert Thomas
Publisher: Boca Raton, FL : CRC Press, 2018. ©2018
Series: Practical spectroscopy, v. 40.
Edition/Format:   eBook : Document : English : First editionView all editions and formats
Summary:
"A dedicated guide for the pharmaceutical/nutraceutical QA/QC communities about the new USP Chapters covering metal impurities. It describes the requirements of the new chapters and gives an overview of why the new rules are needed. The fundamental principles and practical benefits of ICP-OES and ICP-MS are covered in a reader-friendly format that a novice in the pharmaceutical and nutraceutical industries will find  Read more...
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Genre/Form: Electronic books
Electronic book
Laboratory Manual
Additional Physical Format: Print version:
Thomas, Robert, 1949-
Measuring elemental impurities in pharmaceuticals.
Boca Raton : CRC Press, Taylor & Francis Group, 2018
(DLC) 2017038198
(OCoLC)1001298247
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: Robert Thomas
ISBN: 9781315271217 1315271214 9781351984409 1351984403 9781138198036 113819803X 1138197963 9781138197961
OCLC Number: 1019658971
Description: 1 online resource.
Contents: Chapter Testing for Heavy Metals --
An ACS Perspective / Thomas Robert --
chapter Elemental Impurities in Pharmaceuticals --
An Overview / Thomas Robert --
chapter An Overview of ICP --
Mass Spectrometry / Thomas Robert --
chapter Principles of Ion Formation / Thomas Robert --
chapter Sample Introduction / Thomas Robert --
chapter Plasma Source / Thomas Robert --
chapter Interface Region / Thomas Robert --
chapter Ion-Focusing System / Thomas Robert --
chapter Mass Analyzers --
Quadrupole Technologya / Thomas Robert --
chapter Mass Analyzers --
Double-Focusing Magnetic Sector Technology / Thomas Robert --
chapter Mass Analyzers --
Time-of-Flight Technology / Thomas Robert --
chapter Mass Analyzers --
Collision/Reaction Cell and Interface Technology / Thomas Robert --
chapter Ion Detectors / Thomas Robert --
chapter Peak Measurement Protocol / Thomas Robert --
chapter Methods of Quantitation / Thomas Robert --
chapter Review of ICP-MS Interferences / Thomas Robert --
chapter Routine Maintenance / Thomas Robert --
chapter Collecting and Preparing the Sample for Analysis / Thomas Robert --
chapter Sample Digestion Techniques for Pharmaceutical Samples / Thomas Robert --
chapter Performance and Productivity Enhancement Techniques / Thomas Robert --
chapter Coupling ICP-MS with Chromatographic Separation Techniques for Speciation Studies / Thomas Robert --
chapter Fundamental Principles, Method Development, and Operational Requirements of ICP-OES / Thomas Robert --
chapter What Atomic Spectroscopic Technique is Right for Your Lab? / Thomas Robert --
chapter Do You Know What It Costs to Run Your Atomic Spectroscopy Instrumentation? / Thomas Robert --
chapter The Risk Assessment Approach / Thomas Robert --
chapter Regulatory Inspection Readiness / Thomas Robert --
chapter How to Select an ICP Mass Spectromete / Thomas Robert --
chapter Plasma Spectrochemistry Glossary of Terms / Thomas Robert --
chapter Useful Contact Information / Thomas Robert.
Series Title: Practical spectroscopy, v. 40.
Responsibility: by Robert Thomas.

Abstract:

"A dedicated guide for the pharmaceutical/nutraceutical QA/QC communities about the new USP Chapters covering metal impurities. It describes the requirements of the new chapters and gives an overview of why the new rules are needed. The fundamental principles and practical benefits of ICP-OES and ICP-MS are covered in a reader-friendly format that a novice in the pharmaceutical and nutraceutical industries will find easy to understand. It includes easy-to-read chapters on hardware components, calibration protocols, typical interferences, routine maintenance and trouble-shooting procedures. Similar guidelines being proposed by the ICH will also be included."--Provided by publisher.

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