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Solid-State NMR in zeolite catalysis

Author: Jun Xu; Qiang Wang; Shenhui Li; Feng Deng
Publisher: Singapore : Springer, [2019] ©2019
Series: Lecture notes in chemistry, 103.
Edition/Format:   eBook : Document : EnglishView all editions and formats
Summary:
Solid-State NMR Characterization of Heterogeneous Catalysts and Catalytic Reactions provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these techniques in heterogeneous catalysts and related catalytic reactions. It includes an introduction to the basic theory of solid-state NMR and various frequently used techniques. Special emphasis is placed on characterizing the  Read more...
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Genre/Form: Electronic books
Additional Physical Format: Printed edition:
Printed edition:
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: Jun Xu; Qiang Wang; Shenhui Li; Feng Deng
ISBN: 9789811369674 9811369674 9811369658 9789811369650 9789811369667 9811369666
OCLC Number: 1101101086
Description: 1 online resource
Contents: Intro; Preface; Contents; 1 Solid-State NMR Principles and Techniques; 1.1 Introduction; 1.2 Nuclear Spin Interactions in Solids; 1.2.1 Chemical Shift Interaction; 1.2.2 Dipole-Dipole Interaction; 1.2.3 Quadrupolar Interaction; 1.2.4 Spin-Spin Interaction; 1.3 Manipulations of Spin Interactions in Solids; 1.3.1 Magic-Angle Spinning (MAS); 1.3.2 Cross-Polarization; 1.3.3 Dipolar Decoupling Methods in Rotating Solid; 1.3.4 Dipolar Recoupling Methods in Rotating Solid; 1.3.5 High-Resolution Techniques for Half-Integer-Spin Quadrupolar Nuclei; 1.3.6 Summary; References 2 Solid-State NMR Studies of Zeolites and Zeotype Materials Synthesis2.1 Introduction; 2.2 Zeolite Synthesis Route and Procedures; 2.3 Zeolite Synthesis Process and Crystallization Mechanism; 2.4 NMR Strategy in Characterization of Zeolite Synthesis; 2.4.1 Microporous Aluminosilicates; 2.4.2 Microporous Aluminophosphates; 2.5 Summary; References; 3 Solid-State NMR Characterization of Framework Structure of Zeolites and Zeotype Materials; 3.1 Introduction; 3.2 Solid-State NMR Characterization of Zeolite Framework Structure; 3.2.1 27Al MAS NMR; 3.2.2 29Si MAS NMR; 3.2.3 31P MAS NMR 3.2.4 17O MAS NMR3.2.5 129Xe NMR; 3.2.6 Other Framework Elements; 3.3 Summary; References; 4 Solid-State NMR Characterization of Host-Guest Interactions; 4.1 Introduction; 4.2 Solid-State NMR Characterization of Host-Guest Interactions; 4.2.1 Host-Guest Interaction Between Adsorbed Molecule and Zeolite Framework; 4.2.2 Host-Guest Interaction in Molecular Sieve Synthesis; 4.2.3 Host-Guest Interaction in Zeolite Catalysis; 4.3 Summary; References; 5 Solid-State NMR Characterization of Acid Properties of Zeolites and Solid Acid Catalysts; 5.1 Introduction 5.2 Solid-State NMR Characterization of Acidic Property5.2.1 Acid Sites Containing Hydroxyl Groups; 5.2.2 Acidic Nature and Strength; 5.2.3 Location and Distribution of Acid Sites; 5.2.4 Spatial Proximities and Synergy Effects of Different Acid Sites; 5.3 Summary; References; 6 In Situ Solid-State NMR Investigation of Catalytic Reactions on Zeolites; 6.1 Introduction; 6.2 In Situ Solid-State NMR Approaches; 6.2.1 Batch Reaction; 6.2.2 Flow Reaction; 6.3 Mechanistic Study of the Catalytic Reactions by In Situ NMR; 6.3.1 Activation and Conversion of Light Alkanes 6.3.2 Methanol-to-Olefins (MTO) Conversion6.4 Summary; References; Index
Series Title: Lecture notes in chemistry, 103.
Responsibility: Jun Xu, Qiang Wang, Shenhui Li and Feng Deng.

Abstract:

Solid-State NMR Characterization of Heterogeneous Catalysts and Catalytic Reactions provides a comprehensive account of state-of-the-art solid-state NMR techniques and the application of these  Read more...

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