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Transition metal-dinitrogen complexes : preparation and reactivity

Author: Yoshiaki Nishibayashi
Publisher: Weinheim, Germany : Wiley-VCH Verlag GmbH & Co., [2019] ©2019
Edition/Format:   eBook : Document : EnglishView all editions and formats
Summary:
A comprehensive book that explores nitrogen fixation by using transition metal-dinitrogen complexes Nitrogen fixation is one of the most prominent fields of research in chemistry. This book puts the focus on the development of catalytic ammonia formation from nitrogen gas under ambient reaction conditions that has been recently repowered by some research groups. With contributions from noted experts in the field,  Read more...
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Genre/Form: Electronic books
Additional Physical Format: Print version:
Transition metal-dinitrogen complexes.
Weinheim, Germany : Wiley-VCH Verlag GmbH & Co., [2019]
(OCoLC)1031460709
Material Type: Document, Internet resource
Document Type: Internet Resource, Computer File
All Authors / Contributors: Yoshiaki Nishibayashi
ISBN: 9783527344260 3527344268
OCLC Number: 1083522400
Description: 1 online resource
Contents: Preface xiAbout the Editor xiii1 Overviews of the Preparation and Reactivity of Transition Metal-Dinitrogen Complexes 1Yoshiaki Tanabe and Yoshiaki Nishibayashi1.1 Introduction 11.2 Biological Nitrogen Fixation 41.3 Historical Background of Transition Metal-Dinitrogen Complexes 91.4 Coordination Chemistry of Transition Metal-Dinitrogen Complexes 131.4.1 Coordination Patterns of Dinitrogen and Mononuclear Transition Metal-Dinitrogen Complexes 131.4.2 Multinuclear Transition Metal-Dinitrogen Complexes 161.5 Chemical Activation and Reactivity of Dinitrogen Using Transition Metal Complexes 211.5.1 Protonation of Transition Metal-bound Dinitrogen 211.5.2 Cleavage of Transition Metal-bound Dinitrogen 251.5.3 Reaction of Transition Metal-bound Dinitrogen with Dihydrogen 261.5.4 Functionalization of Transition Metal-bound Dinitrogen 291.5.5 Electrochemical and Photochemical Conversion of Dinitrogen Using Transition Metal Complexes 311.6 Catalytic Conversion of Dinitrogen into Ammonia Using Transition Metal Complexes 341.6.1 Catalytic Formation of Ammonia or Hydrazine Using Molybdenum Complexes 341.6.2 Catalytic Formation of Ammonia or Hydrazine Using Transition Metal Other than Molybdenum (Iron, Ruthenium, Osmium, Cobalt, and Vanadium) Complexes 401.6.3 Catalytic Transformation of Hydrazine into Ammonia 451.6.4 Catalytic Formation of Silylamine 471.7 Conclusion and Perspectives 50References 512 Group 4 Transition Metal-Dinitrogen Complexes 79Hidetake Seino and Yuji Kajita2.1 Introduction 792.2 Preparation of Group 4 Transition Metal-Dinitrogen Complexes 802.2.1 Dinitrogen Complexes of Bis(cyclopentadienyl)titanium Derivatives 802.2.2 Dinitrogen Complexes of Bis(cyclopentadienyl)zirconium and Bis(cyclopentadienyl)hafnium Derivatives 892.2.3 Other Dinitrogen Complexes Based on Cyclopentadienyl Ligands 982.2.4 Dinitrogen Complexes Supported by -donor Ligands 1002.2.5 Heterobimetallic Dinitrogen Complexes 1092.3 Reactions of Group 4 Transition Metal-Dinitrogen Complexes 1122.3.1 Protonation 1122.3.2 Reduction 1152.3.3 Reactions with Hydrogen 1202.3.4 Reactions with Si-H and B-H Bonds 1292.3.5 Reactions with Alkyl Halides and Their Equivalents 1312.3.6 Reactions with Alkynes 1362.3.7 Reactions with Carbon Dioxide and Cumulenes 1382.3.8 Reactions with Carbon Monoxide 1422.3.9 Dinitrogen Ligand Substitution 1482.4 Conclusion and Perspectives 1512.5 Addition After Acceptance of this Manuscript 151References 1523 Group 5 Transition Metal-Dinitrogen Complexes 159Leila M. Duman and Lawrence R. Sita3.1 Introduction 1593.2 Preparation of Group 5 Metal N2 Complexes 1603.2.1 Vanadium 1603.2.2 Niobium 1743.2.3 Tantalum 1783.3 N N Bond CleavageWithin Group 5 Metal N2 Complexes 1873.3.1 Vanadium 1883.3.2 Niobium 1923.3.3 Tantalum 1973.4 Nitrogen Fixation Mediated by Group 5 Transition-metal N2 Complexes 2013.4.1 Vanadium 2023.4.2 Niobium 2043.4.3 Tantalum 2063.5 CPAM Group 5 Bimetallic ( - 1: 1-N2) Complexes 2063.6 Conclusions and Perspectives 212References 2144 Group 6 Transition Metal-Dinitrogen Complexes 221NicolasMezailles4.1 Introduction 2214.2 Preparation of Group 6 Transition Metal-Dinitrogen Complexes 2224.2.1 End-on Dinitrogen Complexes from N2 2224.2.1.1 Arene and Phosphine Ligands 2224.2.1.2 Thioether Ligands 2264.2.1.3 Nitrogen and Cp Ligands 2264.2.2 End-on Bridging Dinitrogen Complexes from N2: Synthesis and N2 Splitting 2284.3 Stoichiometric Reactions of Group 6 Transition Metal-Dinitrogen and Metal-Nitrido Complexes 2344.3.1 N-H Bond Formation 2344.3.2 N-C Bond Formation 2384.3.3 N-element Bond Formation 2414.4 Catalytic Reactions of Group 6 Transition Metal-Dinitrogen Complexes 2474.4.1 Catalytic Formation of N2H4/NH3 from NonisolatedM-N2 Complexes 2474.4.2 Catalytic Formation of N(SiMe3)3 2474.4.3 Catalytic Formation of NH3 2514.5 Chemistry of Cr Complexes 2594.6 Conclusion and Perspectives 261References 2635 Toward N-NBond Cleavage: Synthesis and Reactivity of Group 7 Dinitrogen Complexes 271Elon A. Ison5.1 Synthesis of Group VII N2 Complexes 2715.1.1 Syntheses of Terminal N2 Complexes 2715.1.2 Reactivity of Terminal N2 Complexes 2755.1.2.1 Synthesis of Bridged N2 Complexes by Reaction with Lewis Acids 2765.1.2.2 Alternative Syntheses of Bridged N2 Complexes 2795.2 Cleavage and Functionalization of N2 Bonds 2805.2.1 Generation of Diazomethane from CpMn(CO)2N2 2805.2.2 Cleavage of N2 in the Coordination Sphere of Rhenium 2815.3 Conclusions and Future Outlook 281References 2826 Group 8 Transition Metal-Dinitrogen Complexes 285Adam D. Piascik and Andrew E. Ashley6.1 Introduction 2856.2 Preparation of Group 8 Transition Metal-Dinitrogen Complexes 2886.2.1 Ligand Substitution 2886.2.2 Precursor Reduction 2926.2.3 Other Methods 2966.3 Stoichiometric Reactions of Group 8 Transition Metal-Dinitrogen Complexes 2976.3.1 Substitution Reactions and Lability of Bound N2 2976.3.2 Cleavage and Functionalization of Coordinated N2 3016.3.3 Other Stoichiometric Reactivity 3096.4 Catalytic Reactions of Group 8 Transition Metal-Dinitrogen Complexes 3116.4.1 Early Results and Fe Bis(diphosphine) Systems for Catalytic N2 Fixation 3116.4.2 Catalytic NH3 Production by EPR 3-supported Systems 3136.4.3 Catalytic N2 Fixation by Other Systems 3176.4.4 Other Catalytic Reactions of Group 8 M-N2 Complexes 3196.5 Conclusion and Perspectives 327References 3287 Group 9 Transition Metal-Dinitrogen Complexes 337Connie C. Lu and Steven D. Prinslow7.1 Cobalt-Dinitrogen Complexes 3377.1.1 Monodentate Phosphine Donors 3387.1.1.1 CoH(N2)(PR3)3 and Related Co(I) Complexes 3387.1.1.2 Cobaltate Complexes: [Co(N2)(PR3)3] 3427.1.2 Tripodal Polyphosphine Ligands 3457.1.2.1 Tris(phosphine) Ligands 3457.1.2.2 Tris(phosphino)borate Ligands 3467.1.2.3 Trisphosphine Systems with an Apical Main Group Donor 3477.1.2.4 Trisphosphine Systems with an Apical Transition Metalloligand Donor 3507.1.3 Ligands with Exclusively Nitrogen Donors 3557.1.3.1 Tris(pyrazoyl)borate (Tp) Ligands 3557.1.3.2 -diketiminate Ligands 3567.1.3.3 Bis( -imino)pyridine Ligands 3587.1.4 N-heterocyclic Carbene Ligands 3597.1.5 Pincer Ligands 3607.1.5.1 Monoanionic PNP-Type and PBP-Type Ligands 3617.1.5.2 Pincer Ligands with N/P Donors 3637.1.5.3 N-heterocyclic Carbene-Based Pincer Ligands 3657.1.6 Other Assorted Ligands 3677.1.7 Analysis and Summary of Cobalt-Dinitrogen Complexes 3697.2 Rhodium-Dinitrogen Complexes 3707.2.1 Early Rh-N2 Complexes 3707.2.2 Phosphine Ligands 3727.2.3 Ligands with Exclusively Nitrogen Donors 3747.2.3.1 Bis( -imino)pyridine Ligands 3747.2.3.2 -diketiminate Ligands 3757.2.4 Pincer Ligands 3757.2.4.1 PCP Pincer Ligands 3767.2.4.2 PNP Pincer Ligands 3787.2.4.3 Other Pincer Ligands 3807.2.5 N-heterocyclic Carbene Ligands 3807.2.6 Summary of Rhodium-Dinitrogen Complexes 3817.3 Iridium-Dinitrogen Complexes 3817.3.1 Early Ir-N2 Complexes 3827.3.2 Phosphine Ligands 3837.3.3 Ligands with Exclusively Nitrogen Donors 3857.3.3.1 Tris(pyrazoyl)borate (Tp) Ligands 3857.3.3.2 -diketiminate Ligands 3867.3.4 Pincer Ligands 3867.3.4.1 PNP-Type Pincer Ligands 3867.3.4.2 PCP- and PSiP-Type Pincer Ligands 3887.3.5 N-heterocyclic Carbene Ligands 3907.3.6 Miscellaneous 3917.3.7 Summary of Iridium-Dinitrogen Complexes 3917.4 Group 9 Catalysts for N2 Functionalization 3927.4.1 Cobalt-Based Catalysts 3927.4.1.1 Dinitrogen Silylation 3937.4.1.2 Dinitrogen Fixation 3957.4.2 Outlook for Rhodium and Iridium Catalysts 396Acknowledgments 396References 3968 Group 10 and 11 Transition Metal-Dinitrogen Complexes 403Ricardo B. Ferreira and Leslie J. Murray8.1 Introduction 4038.2 Group 10 Transition Metal-Dinitrogen Complexes 4058.2.1 Nickel 4058.2.1.1 Interaction of Dinitrogen with Nickel Surfaces 4068.2.1.2 Matrix-Assisted Isolation of Binary or Ternary Compounds 4068.2.1.3 Coordination Compounds 4088.2.1.4 Structural Relationships and Comparisons 4208.2.2 Palladium and Platinum 4228.3 Group 11 Transition Metal-Dinitrogen Complexes 4238.3.1 Copper 4238.3.1.1 Matrix-Assisted Isolation of Binary or Ternary Compounds 4238.3.1.2 Coordination Compounds 4258.3.1.3 Structural Relationships and Comparisons 4278.3.2 Silver and Gold 4298.4 Conclusion and Perspectives 430References 4319 Group 3 Transition Metal, Lanthanide, and Actinide-Dinitrogen Complexes 441Yoshiaki Tanabe9.1 Introduction 4419.2 Preparation and Characterization of Group 3 Transition Metal, Lanthanide, and Actinide-Dinitrogen Complexes 4439.2.1 Overviews of Preparation, Structures, and Characterization of Group 3 Transition Metal, Lanthanide, and Actinide-Dinitrogen Complexes 4439.2.2 Preparation and Structures of Side-on-Bound {(N2)2 }-Bridged Dinuclear Group 3 Transition Metal, Lanthanide, and Actinide-Dinitrogen Complexes 4439.2.3 Preparation and Structures of Side-on-bound {(N2)3 }-Bridged Dinuclear Group 3 Transition Metal and Lanthanide Complexes 4569.2.4 Preparation and Structures of {(N2)4 }-Bridged Dinuclear, Trinuclear, and Tetranuclear Lanthanide and Actinide-Dinitrogen Complexes 4579.2.5 Preparation and Structures of End-on-Bound Group 3 Transition Metal, Lanthanide, and Actinide-Dinitrogen Complexes 4609.3 Reactivity and Property of Group 3 Transition Metal, Lanthanide, and Actinide-Dinitrogen Complexes 4629.3.1 Cleavage, Protonation, and Functionalization of Dinitrogen upon Group 3 Transition Metal, Lanthanide, and Actinide-Dinitrogen Complexes 4629.3.2 Group 3 Transition Metal-Dinitrogen Complexes as Mediators for the Transformation of Small Molecules 4669.3.3 {(N2)3 }-Bridged Dinuclear Group 3 Transition Metal and Lanthanide Complexes as Single-Molecule Magnets 4689.4 Conclusion and Perspectives 469References 470Index 475
Responsibility: edited by Yoshiaki Nishibayashi.

Abstract:

A comprehensive book that explores nitrogen fixation by using transition metal-dinitrogen complexes Nitrogen fixation is one of the most prominent fields of research in chemistry. This book puts the focus on the development of catalytic ammonia formation from nitrogen gas under ambient reaction conditions that has been recently repowered by some research groups. With contributions from noted experts in the field, Transition Metal-Dinitrogen Complexes offers an important guide and comprehensive resource to the most recent research and developments on the topic of nitrogen fixation by using transition metal-dinitrogen. The book is filled with the information needed to understand the synthesis of transition metal-dinitrogen complexes and their reactivity. This important book: -Offers a resource for understanding nitrogen fixation chemistry that is essential for explosives, pharmaceuticals, dyes, and all forms of life -Includes the information needed for anyone interested in the field of nitrogen fixation by using transition metal-dinitrogen complexes -Contains state-of-the-art research on synthesis of transition metal-dinitrogen complexes and their reactivity in nitrogen fixation -Incorporates contributions from well-known specialists and experts with an editor who is an innovator in the field of dinitrogen chemistry Written for chemists and scientists with an interest in nitrogen fixation, Transition Metal-Dinitrogen Complexes is a must-have resource to the burgeoning field of nitrogen fixation by using transition metal-dinitrogen complexes.

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